Sigma 4-16KS Operating Manual
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Sigma 4-16KS Operating Manual

Refrigerated centrifuge
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Translation of the original operating manual
sb
Sigma
Донау Лаб. Москва/ «Donau Lab. Moscow» - официальный дистрибьютер оборудования
07/2012
www.donaulab.ru
Тел. +7 (495)-255-33-89
Адрес: 11
9034, Москва, Турчанинов пер,
д.6,
стр.2
Rev. 1.11 of 06/11/2015
Sigma 4-16KS; ;
part no. 07057
Sigma 4-16KS
from serial no. 144061
Refrigerated Centrifuge
Operating Manual
Please retain for later use!

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  • Page 1 Донау Лаб. Москва/ «Donau Lab. Moscow» - официальный дистрибьютер оборудования 07/2012 www.donaulab.ru Тел. +7 (495)-255-33-89 Адрес: 11 9034, Москва, Турчанинов пер, д.6, стр.2 Rev. 1.11 of 06/11/2015 Sigma 4-16KS; ; part no. 07057 Sigma 4-16KS from serial no. 144061 Refrigerated Centrifuge Operating Manual Please retain for later use!
  • Page 2 Refrigerated Centrifuge Sigma 4-16KS Version 07/2012, Rev. 1.11 of 06/11/2015 • sb Translation of the original operating manual, part no. 07057...
  • Page 3 Refrigerated Centrifuge Sigma 4-16KS In case of inquiries, please state the following numbers: Order number: Serial number: © Copyright by Sigma Laborzentrifugen GmbH An der Unteren Söse 50 37520 Osterode am Harz Germany Tel.: +49 (0) 5522 / 5007-0 Fax: +49 (0) 5522 / 5007-12 Web: www.sigma-zentrifugen.de...
  • Page 4 Refrigerated Centrifuge Sigma 4-16KS Version 07/2012, Rev. 1.11 of 06/11/2015 • sb Translation of the original operating manual, part no. 07057...
  • Page 5 Refrigerated Centrifuge Sigma 4-16KS Table of contents General information ......................9 Importance of the operating manual .................. 9 Intended use ........................9 Warranty and liability ......................9 Copyright ........................10 Standards and regulations ....................10 Scope of supply ......................10 Layout and mode of operation ..................
  • Page 6 Refrigerated Centrifuge Sigma 4-16KS Table of contents Storage and transport ....................... 24 Dimensions and weight ....................24 Storage conditions ......................24 Notes on transport ......................24 Packaging ........................25 Transport safety device ....................25 Set-up and connection ...................... 26 Installation site ........................ 26 Power supply ........................
  • Page 7 Refrigerated Centrifuge Sigma 4-16KS Table of contents Malfunctions and error correction ..................55 General malfunctions ...................... 55 7.1.1 Emergency lid release ....................56 Table of error codes ......................57 Service contact ....................... 58 Maintenance and service....................59 Maintenance ........................59 8.1.1...

  • Page 8: Translation Of The Original Operating Manual, Part No

    Refrigerated Centrifuge Sigma 4-16KS Table of contents Version 07/2012, Rev. 1.11 of 06/11/2015 • sb Translation of the original operating manual, part no. 07057...

  • Page 9: General Information

    They are solely intended for this purpose. Any other use beyond this area of application is regarded as improper use. Sigma Laborzentrifugen GmbH cannot be held liable for any damage resulting from such improper use.

  • Page 10: Copyright

    Pos: 12 / 100 Sigma /110 BA Ze ntrifu gen Sigma (Proj ekte )/4- 16KS_4 -16KHS/0 10 Allge mein e In for matio nen 010 -00 60 Li efe rum fang 4- 16KS_KHS @ 2 9\m od_1 405 326 882 555 _68.

  • Page 11: Layout And Mode Of Operation

    Pos: 17 / 100 Sigma /110 BA Ze ntrifu gen Sigma (Proj ekte )/4- 16KS_4 -16KHS/0 20 Auf bau und Wirku ngsweis e02 0-0 010 -00 10 Funkti ons- un d Bedie nele men te 4 -16KS @ 29\ mod _14 053 268 9040 6_6 8.d...

  • Page 12: Name Plate

    Pos: 19 / 100 Sigma /110 BA Ze ntrifu gen Sigma (Proj ekte )/4- 16KS_4 -16KHS/0 20 Auf bau und Wirku ngsweis e02 0-0 010 -00 20 Type nschild 4-1 6KS @ 29 \mo d_1 405 326 893 261 _68.

  • Page 13: Mode Of Operation

    Pos: 24 / 100 Sigma /100 BA Ze ntrifu gen Sigma (Stan da rdm odule )/0 20 Auf bau und Wirku ngsweis e02 0-0 020 -00 20 Anw end ungs ber eich @ 26\ mo d_1 4053 189 867 63_ 68.d...

  • Page 14: Speed, Radius, And Relative Centrifugal Force

    Pos: 28 / 100 Sigma /100 BA Ze ntrifu gen Sigma (Stan da rdm odule )/0 20 Auf bau und Wirku ngsweis e02 0-0 020 -00 20- 002 0 Dich te @ 26\ mod _14 0531 898 935 9_6 8.do...

  • Page 15: Safety

    Pos: 32 / 100 Sigma /100 BA Ze ntrifu gen Sigma (Stan da rdm odule )/0 30 Sich erh eit03 0-0 010 Beschild er ung des G erä ts @ 30\m od_ 140 540 400 247 7_6 8.docx...

  • Page 16: Explanation Of The Symbols And Notes

    Refrigerated Centrifuge Sigma 4-16KS 3 Safety Explanation of the symbols and notes In this operating manual, the following names and symbols to indicate hazards are used: This symbol stands for a direct hazard to the life and health of persons.

  • Page 17: Responsibility Of The Operator

    Pos: 38 / 100 Sigma /100 BA Ze ntrifu gen Sigma (Stan da rdm odule )/0 30 Sich erh eit03 0-0 040 Bedie npe rson al @ 26\ mod_ 140 531 901 763 4_6 8.docx...

  • Page 18: Safety Instructions

    Pos: 43 / 100 Sigma /100 BA Ze ntrifu gen Sigma (Stan da rdm odule )/0 30 Sich erh eit03 0-0 060 -00 10 Ele ktrisch e Siche rheit @ 2 6\m od_ 1405 319 022 891 _68.

  • Page 19: Fire Prevention

    Pos: 49 / 100 Sigma /100 BA Ze ntrifu gen Sigma (Stan da rdm odule )/0 30 Sich erh eit03 0-0 060 -00 40 C he mische und biolo gische Sicher heit @ 26\ mod _14 053 190 281 41_ 68.d...

  • Page 20: Safety Instructions For Centrifugation

    Pos: 53 / 100 Sigma /100 BA Ze ntrifu gen Sigma (Stan da rdm odule )/0 30 Sich erh eit03 0-0 060 -00 60 B estän digkeit von K unstst offe n @ 2 6\m od_ 140 531 903 1161 _68 .docx...

  • Page 21: Service Life Of Rotors And Accessories

    Pos: 55 / 100 Sigma /100 BA Ze ntrifu gen Sigma (Stan da rdm odule )/0 30 Sich erh eit03 0-0 060 -00 70 Leb ensd aue r vo n Rot ore n un d Z ube hör...

  • Page 22: Safety Devices

    Pos: 58 / 100 Sigma /100 BA Ze ntrifu gen Sigma (Stan da rdm odule )/0 30 Sich erh eit03 0-0 070 -00 10 D eckelv erri egelu ng @ 27\ mo d_14 053 190 363 21_ 68.d...

  • Page 23: Measures In The Event Of Hazards And Accidents

    Pos: 73 / 100 Sigma /100 BA Ze ntrifu gen Sigma (Stan da rdm odule )/0 30 Sich erh eit03 0-0 090 Rest risiken @ 2 7\mo d_1 405 319 052 885 _68.

  • Page 24: Storage And Transport

    Pos: 79 / 100 Sigma /100 BA Ze ntrifu gen Sigma (Stan da rdm odule )/0 40 L age run g u nd Tra nspo rt04 0- 0020 L age rbe dingu nge n @ 27\m od_ 140 531 916 144 2_6 8.docx...

  • Page 25: Packaging

    Pos: 83 / 100 Sigma /110 BA Ze ntrifu gen Sigma (Proj ekte )/4- 16KS_4 -16KHS/0 40 L age run g u nd Tra nspo rt04 0-0 040 Verp acku ng 4 -16KS_KHS @ 29\ mod _140 532 691 375 2_6 8.doc...

  • Page 26: Set-Up And Connection

    Pos: 90 / 100 Sigma /100 BA Ze ntrifu gen Sigma (Stan da rdm odule )/0 50 Aufs tellun g u nd Ansc hluss0 50- 001 0 Aufs tellor t @ 2 7\m od_ 140 531 917 4276 _68 .docx...

  • Page 27: Using The Centrifuge

    Pos: 99 / 100 Sigma /100 BA Ze ntrifu gen Sigma (Stan da rdm odule )/0 60 Bet rieb _Spinco ntr ol L+S 060 -001 0 Er ste I nbet rieb nah me @ 27\ mo d_14 053 192 001 30_ 68.d...

  • Page 28: Installation Of Angle Rotors With A Hermetically Sealed Lid

    Refrigerated Centrifuge Sigma 4-16KS 6 Using the centrifuge When using rotors for microtiter plate formats: Ensure that the plate holders are inserted together with the plates into the buckets. CAUTION The lid screw serves for the fastening of the lid onto the rotor only, not for the fastening of the rotor onto the motor shaft.

  • Page 29: Installation Of Accessories

    Refrigerated Centrifuge Sigma 4-16KS 6 Using the centrifuge Pos: 110 /10 0 Sigm a/10 0 BA Z entrif uge n Sigm a (Sta nda rd mod ule)/ 060 B etrie b_Spinc ont rol L +S060 -00 20 -002 0-0 032 Einset zen v on Zub ehö r 4 +6pl ätzig 4 -1 6S bis 6 -16KS @ 27\ mod _14 0531 920 770 9_6 8.do cx @ 1 925 35 @ 4 @ 1 6.2.2.3...
  • Page 30 Refrigerated Centrifuge Sigma 4-16KS 6 Using the centrifuge Centrifugation with low capacity • Install the tubes axial symmetrically so that the buckets and their inserts are loaded evenly. • It is not permissible to load angle rotors on only one axis.

  • Page 31: Adapters

    Refrigerated Centrifuge Sigma 4-16KS 6 Using the centrifuge Pos: 112 /10 0 Sigm a/10 0 BA Z entrif uge n Sigm a (Sta nda rd mod ule)/ 060 B etrie b_Spinc ont rol L +S060 -00 20 -002 0-0 040 Ada pter - nur L+S @ 27\ mod _14 053 192 1019 1_6 8.d ocx @ 1925 63 @ 4 @ 1 6.2.2.4...

  • Page 32: Control System "Spincontrol S

    Refrigerated Centrifuge Sigma 4-16KS 6 Using the centrifuge Pos: 116 /10 0 Sigm a/10 0 BA Z entrif uge n Sigm a (Sta nda rd mod ule)/ 060 B etrie b_Spinc ont rol L +S/Spinco ntr ol S ( Zent 7)0 60- 003 0 Spin cont rol S Ste uer ung --- -- --- -- --- --- -- --- -- --- -- --- --- -- --- -- --- -- @ 27\ mo d_14 053 201 923 64_ 68.d ocx @ 193 109 @ 2 @ 1 Control system "Spincontrol S"...

  • Page 33: Manual Mode

    Refrigerated Centrifuge Sigma 4-16KS 6 Using the centrifuge Pos: 119 /10 0 Sigm a/10 0 BA Z entrif uge n Sigm a (Sta nda rd mod ule)/ 060 B etrie b_Spinc ont rol L +S/Spinco ntr ol S ( Zent 7)0 60- 003 0-0 020 M anu eller Bet rieb @ 2 7\m od_1 405 320 198 028 _68. docx @ 19 315 1 @ 3 @ 1 6.3.2...

  • Page 34: Standard Menu

    Refrigerated Centrifuge Sigma 4-16KS 6 Using the centrifuge Pos: 128 /10 0 Sigm a/10 0 BA Z entrif uge n Sigm a (Sta nda rd mod ule)/ 060 B etrie b_Spinc ont rol L +S/Spinco ntr ol S ( Zent 7)0 60- 003 0-0 020 -00 50 Me nü Sta nda rd - nur KS @ 27 \mo d_1 405 3202 040 84_ 68.d ocx @ 193 221 @ 4 @ 1 6.3.2.5...
  • Page 35 Refrigerated Centrifuge Sigma 4-16KS 6 Using the centrifuge Runtime The set runtime is displayed in the upper section of this field, with the remaining runtime shown below. The runtime is defined as the period from the start of the centrifuge to the beginning of the deceleration phase. The maximum value is 99 h 59 min 59 sec.
  • Page 36 Refrigerated Centrifuge Sigma 4-16KS 6 Using the centrifuge Rotor: rotor selection list This field shows the rotor that is currently being used. • Select the field "Rotor" and confirm the selection. A list with all of the possible rotors without buckets is displayed.
  • Page 37 Refrigerated Centrifuge Sigma 4-16KS 6 Using the centrifuge Acceleration This function is used to select an acceleration curve. One can select a linear rise (curves 0-9) or a quadratic rise (curves 10-19). The acceleration curves 20-29 can be programmed as desired (see chapter 11.3 - "Acceleration and deceleration curves").
  • Page 38 Refrigerated Centrifuge Sigma 4-16KS 6 Using the centrifuge Fig. 14: Program "RAPID_TEMP" The program will only be loaded if the actual temperature is above the set temperature. NOTE • Press the start button in order to start the rapid cooling run.
  • Page 39 Refrigerated Centrifuge Sigma 4-16KS 6 Using the centrifuge If the "RAPID_TEMP" program is used, the temperature of the unloaded aluminium bucket will be displayed. If samples, which have not been precooled, are placed into the buckets, the displayed temperature will deviate from the actual sample temperature.

  • Page 40: Process Library Menu

    Refrigerated Centrifuge Sigma 4-16KS 6 Using the centrifuge Pos: 130 /10 0 Sigm a/10 0 BA Z entrif uge n Sigm a (Sta nda rd mod ule)/ 060 B etrie b_Spinc ont rol L +S/Spinco ntr ol S ( Zent 7)0 60- 003 0-0 020 -00 55 Me nü Pro zessbi blioth ek @ 27\m od_ 140 532 020 912 3_68 .docx @ 1 932 76 @ 4 @ 1 6.3.2.6...

  • Page 41: Parameters Menu

    Refrigerated Centrifuge Sigma 4-16KS 6 Using the centrifuge Pos: 132 /10 0 Sigm a/10 0 BA Z entrif uge n Sigm a (Sta nda rd mod ule)/ 060 B etrie b_Spinc ont rol L +S/Spinco ntr ol S ( Zent 7)0 60- 003 0-0 020 -00 60 Me nü Par am eter - n ur KS @ 27\ mod _14 053 2021 864 0_6 8.d ocx @ 1933 05 @ 4 @ 1 6.3.2.7...
  • Page 42 Refrigerated Centrifuge Sigma 4-16KS 6 Using the centrifuge Density This setting is useful for glass vessels. If the density of the liquid to be centrifuged is higher than 1.2 g/cm , the value must be adapted manually in order to prevent the glass vessel from breaking. This will reduce the maximum possible final speed (see chapter 2.2.2.2 - "Density").
  • Page 43 Refrigerated Centrifuge Sigma 4-16KS 6 Using the centrifuge Temperature monitoring The control system includes a temperature monitoring function. If the actual temperature difference with regard to the set value deviates from the set temperature difference, the centrifuge will stop and an error message will be issued.
  • Page 44 Refrigerated Centrifuge Sigma 4-16KS 6 Using the centrifuge Lock In order to prevent any unauthorised use of the centrifuge, the following functions can be blocked: • Saving of programs (level 01) • Changing of parameters, short run (level 02) •...

  • Page 45: Setup Menu

    Refrigerated Centrifuge Sigma 4-16KS 6 Using the centrifuge Pos: 134 /10 0 Sigm a/10 0 BA Z entrif uge n Sigm a (Sta nda rd mod ule)/ 060 B etrie b_Spinc ont rol L +S/Spinco ntr ol S ( Zent 7)0 60- 003 0-0 020 -00 70 Me nü Set up @ 27\ mod _14 053 2022 547 9_6 8.d ocx @ 1933 61 @ 4 @ 1 6.3.2.8...
  • Page 46 Refrigerated Centrifuge Sigma 4-16KS 6 Using the centrifuge Start delay If the start delay function is active, the centrifuge will not start until the preset time has elapsed. The symbol " " will be displayed in the runtime field. Display deceleration time In the activated mode, the deceleration time will be displayed instead of the runtime during and after the deceleration process.
  • Page 47 Refrigerated Centrifuge Sigma 4-16KS 6 Using the centrifuge System Cycles This field shows the number of cycles as well as the runtime of the rotor and buckets that are used. Info This item provides information on the software versions that are used in this centrifuge.

  • Page 48: Curve Menu

    Refrigerated Centrifuge Sigma 4-16KS 6 Using the centrifuge Pos: 136 /10 0 Sigm a/10 0 BA Z entrif uge n Sigm a (Sta nda rd mod ule)/ 060 B etrie b_Spinc ont rol L +S/Spinco ntr ol S ( Zent 7)0 60- 003 0-0 020 -00 80 Me nü Kur ve @ 27\ mod _14 053 2022 816 9_6 8.d ocx @ 1933 89 @ 4 @ 1 6.3.2.9...

  • Page 49: Help Menu

    Refrigerated Centrifuge Sigma 4-16KS 6 Using the centrifuge Restrictions • Acceleration and deceleration curves can include intervals with a positive slope as well as intervals with a negative slope and also intervals with 0 slope. • The slope of the curve intervals can be 1 min...

  • Page 50: Changing The Contrast

    Refrigerated Centrifuge Sigma 4-16KS 6 Using the centrifuge Pos: 140 /10 0 Sigm a/10 0 BA Z entrif uge n Sigm a (Sta nda rd mod ule)/ 060 B etrie b_Spinc ont rol L +S/Spinco ntr ol S ( Zent 7)0 60- 003 0-0 020 -01 00 K ontr astä nde run g @ 2 7\m od_ 140 532 0232 376 _68 .docx @ 1 9343 1 @ 4 @ 1 6.3.2.11 Changing the contrast...

  • Page 51: Saving A Program

    Refrigerated Centrifuge Sigma 4-16KS 6 Using the centrifuge Pos: 144 /10 0 Sigm a/10 0 BA Z entrif uge n Sigm a (Sta nda rd mod ule)/ 060 B etrie b_Spinc ont rol L +S/Spinco ntr ol S ( Zent 7)0 60- 003 0-0 030 -00 10 P rog ram m sp eiche rn @ 27\ mo d_14 053 202 378 32_ 68.d ocx @ 193 487 @ 4 @ 1 6.3.3.1...

  • Page 52: Executing A Program

    Refrigerated Centrifuge Sigma 4-16KS 6 Using the centrifuge Fig. 25: Loading a program Pos: 147 /01 0 Univ ersal mod ule/L eerz eile @ 0\m od_ 120 211 624 450 0_0. docx @ 11 4 @ @ 1 Pos: 148 /10 0 Sigm a/10 0 BA Z entrif uge n Sigm a (Sta nda rd mod ule)/ 060 B etrie b_Spinc ont rol L +S/Spinco ntr ol S ( Zent 7)0 60- 003 0-0 030 -00 30 P rog ram m a usfü hre n @ 2 7\m od_ 140 532 0243 642 _68 .docx @ 1 9354 3 @ 4 @ 1 6.3.3.3...

  • Page 53: Automatic Program Rotation

    Refrigerated Centrifuge Sigma 4-16KS 6 Using the centrifuge Pos: 152 /10 0 Sigm a/10 0 BA Z entrif uge n Sigm a (Sta nda rd mod ule)/ 060 B etrie b_Spinc ont rol L +S/Spinco ntr ol S ( Zent 7)0 60- 003 0-0 030 -00 50 A utom atisch e Pro gra mm rota tion @ 27\ mo d_1 4053 202 483 29_ 68.d ocx @ 193 585 @ 4 @ 1 6.3.3.5...

  • Page 54: Options For Data Input And Output

    Refrigerated Centrifuge Sigma 4-16KS 6 Using the centrifuge Pos: 154 /10 0 Sigm a/10 0 BA Z entrif uge n Sigm a (Sta nda rd mod ule)/ 060 B etrie b_Spinc ont rol L +S/Spinco ntr ol S ( Zent 7)0 60- 003 0-0 040 Opti one n zu r Ein- und A usga be vo n Dat en (au ßer 8KS) @ 27\ mod _14 053 202 5148 3_6 8.d ocx @ 1936 13 @ 3 @ 1 6.3.4...

  • Page 55: Translation Of The Original Operating Manual, Part No

    Refrigerated Centrifuge Sigma 4-16KS 7 Malfunctions and error correction Pos: 159 /10 0 Sigm a/10 0 BA Z entrif uge n Sigm a (Sta nda rd mod ule)/ 070 St öru nge n un d Fehle rsuc he0 70 St öru nge n un d F ehle rsuch e= === == == === == == == === == == === == @ 28 \mo d_1 405 320 576 072_ 68. docx @ 19 466 3 @ 1 @ 1 Malfunctions and error correction Pos: 160 /10 0 Sigm a/10 0 BA Z entrif uge n Sigm a (Sta nda rd mod ule)/ 070 St öru nge n un d Fehle rsuc he0 70- 0012 Allge mein e Stör ung en_Spi ncont rol S_ Tr ansp ortsc hra ube n @ 28\m od_ 140 532 057 863 9_68 .docx @ 1 946 91 @ 2 @ 1...

  • Page 56: Emergency Lid Release

    Refrigerated Centrifuge Sigma 4-16KS 7 Malfunctions and error correction Pos: 162 /10 0 Sigm a/11 0 BA Z entrif uge n Sigm a (Pr ojekt e)/4 -16KS_ 4-1 6KHS/070 St öru nge n un d F ehle rsuc he0 70- 0010 -00 10 N oten trie gelun g 4 -16KS_KHS @ 2 9\m od_ 140 532 695 539 0_68 .docx @ 1 987 93 @ 3 @ 1 7.1.1...

  • Page 57: Table Of Error Codes

    Refrigerated Centrifuge Sigma 4-16KS 7 Malfunctions and error correction Pos: 164 /10 0 Sigm a/10 0 BA Z entrif uge n Sigm a (Sta nda rd mod ule)/ 070 St öru nge n un d Fehle rsuc he0 70- 0020 Tabell e de r Fehle rm eldun gen @ 2 8\m od_1 405 320 582 996 _68.

  • Page 58: Service Contact

    Refrigerated Centrifuge Sigma 4-16KS 7 Malfunctions and error correction Pos: 166 /10 0 Sigm a/10 0 BA Z entrif uge n Sigm a (Sta nda rd mod ule)/ 070 St öru nge n un d Fehle rsuc he0 70- 0030 Kon takt i m Servic efall @ 28\ mod _14 053 205 843 61_ 68.d ocx @ 194 775 @ 2 @ 1...

  • Page 59: Maintenance And Service

    Refrigerated Centrifuge Sigma 4-16KS 8 Maintenance and service Pos: 169 /10 0 Sigm a/10 0 BA Z entrif uge n Sigm a (Sta nda rd mod ule)/ 080 W art ung und Inst andh altun g08 0 Wa rtu ng u nd I nsta ndh altun g== == == === == == == === == == === @ 2 8\m od_1 405 320 612 731 _68. docx @ 19 478 9 @ 1 @ 1...

  • Page 60: Condenser (Only Refrigerated Centrifuges)

    Refrigerated Centrifuge Sigma 4-16KS 8 Maintenance and service Pos: 174 /10 0 Sigm a/10 0 BA Z entrif uge n Sigm a (Sta nda rd mod ule)/ 080 W art ung und Inst andh altun g08 0-0 010 -00 10- 001 0 Ko nde nsato r @ 28\ mod _14 0532 061 670 8_6 8.do cx @ 1 948 31 @ 4 @ 1 8.1.2...

  • Page 61: Plastic Accessories

    Refrigerated Centrifuge Sigma 4-16KS 8 Maintenance and service Pos: 178 /10 0 Sigm a/10 0 BA Z entrif uge n Sigm a (Sta nda rd mod ule)/ 080 W art ung und Inst andh altun g08 0-0 010 -00 20- 001 0 Ku nststo ffzub ehö r @ 28\ mod _140 532 061 960 2_6 8.doc x @ 1 948 59 @ 4 @ 1 8.1.3.1...

  • Page 62: Glass Breakage

    Refrigerated Centrifuge Sigma 4-16KS 8 Maintenance and service Pos: 184 /10 0 Sigm a/10 0 BA Z entrif uge n Sigm a (Sta nda rd mod ule)/ 080 W art ung und Inst andh altun g08 0-0 010 -00 60 Glasb ruc h @ 2 8\m od_ 140 532 0623 434 _68 .docx @ 19 490 1 @ 3 @ 1 8.1.6...

  • Page 63: Autoclaving

    Refrigerated Centrifuge Sigma 4-16KS 8 Maintenance and service Pos: 188 /10 0 Sigm a/10 0 BA Z entrif uge n Sigm a (Sta nda rd mod ule)/ 080 W art ung und Inst andh altun g08 0-0 020 -00 10 Autokla viere n @ 28\ mod _140 532 062 744 0_6 8.doc x @ 1 949 43 @ 3 @ 1 8.2.1 Autoclaving...

  • Page 64: Service

    Refrigerated Centrifuge Sigma 4-16KS 8 Maintenance and service Pos: 190 /10 0 Sigm a/10 0 BA Z entrif uge n Sigm a (Sta nda rd mod ule)/ 080 W art ung und Inst andh altun g08 0-0 030 Ins tan dhalt ungs arb eiten @ 2 8\mo d_1 405 320 628 810 _68. docx @ 19 495 7 @ 2 @ 1...

  • Page 65: Return Of Defective Parts

    Refrigerated Centrifuge Sigma 4-16KS 8 Maintenance and service Pos: 192 /10 0 Sigm a/10 0 BA Z entrif uge n Sigm a (Sta nda rd mod ule)/ 080 W art ung und Inst andh altun g08 0-0 040 Rücks end ung def ekte r T eile @ 28\ mod _140 532 063 022 6_6 8.doc x @ 1 949 71 @ 2 @ 1...
  • Page 66 Refrigerated Centrifuge Sigma 4-16KS 8 Maintenance and service The unit must be packaged in a transport-safe manner. Please use the original packaging, if at all possible. If the product is dispatched to us in unsuitable packaging, you will be charged the cost for returning it to you in new packaging.

  • Page 67: Disposal

    Pos: 197 /10 0 Sigm a/10 0 BA Z entrif uge n Sigm a (Sta nda rd mod ule)/ 090 E ntso rgun g09 0-0 010 Ents org ung der Ze ntrif uge --- -- --- -- --- --- -- --- -- --- --- -- --- -- --- -- --- -- @ 28\ mo d_14 053 206 600 29_ 68.d ocx @ 194 999 @ 2 @ 1 Disposal of the centrifuge In accordance with the directive 2002/96/EC, SIGMA centrifuges are marked with the symbol shown to the left. This symbol means that it is not permissible to dispose of the unit among household waste.

  • Page 68: Technical Data

    Refrigerated Centrifuge Sigma 4-16KS 10 Technical data Pos: 202 /10 0 Sigm a/11 0 BA Z entrif uge n Sigm a (Pr ojekt e)/4 -16KS_ 4-1 6KHS/100 Tec hnisch e Dat en1 00 Tech nische Date n 4 -16KS= == === == == === == == === == == === == @ 2 9\mo d_1 405 326 982 149 _68. docx @ 19 882 1 @ 1 @ 1...

  • Page 69: Technical Documentation

    Refrigerated Centrifuge Sigma 4-16KS 10 Technical data 10.2 Technical documentation For environmental reasons, the comprehensive technical documentation of the centrifuge (e.g. circuit diagrams) and the safety data sheets of the manufacturers of refrigerant and lubricants are not attached to this documentation.

  • Page 70: Appendix

    Refrigerated Centrifuge Sigma 4-16KS 11 Appendix Pos: 209 /10 0 Sigm a/10 0 BA Z entrif uge n Sigm a (Sta nda rd mod ule)/ 110 A nha ng11 0 An han g== == == == === == == === == == === == == === == == = @ 2 8\m od_ 140 532 069 931 0_68 .docx @ 1 950 69 @ 1 @ 1 11 Appendix Pos: 210 /10 0 Sigm a/11 0 BA Z entrif uge n Sigm a (Pr ojekt e)/4 -16KS_ 4-1 6KHS/110 A nhan g11 0-0 010 Zu beh örp rog ra mm 4-1 6KS_KHS @ 29\ mod _14 053 270 077 51_ 68.d ocx @ 198 835 @ 2 @ 1...
  • Page 71 Refrigerated Centrifuge Sigma 4-16KS 11 Appendix Part no. Description Max. speed Max. (rpm) gravitational field (x g) 12265 Angle rotor 6 x 85 ml, Biosafe with certificate, for tubes no. 13085, 15076, 15080, incl. bayonet lid no. 17607, Radius max. 10.6 cm, radius min. 3.5 cm, angle 25°...
  • Page 72 Refrigerated Centrifuge Sigma 4-16KS 11 Appendix Part no. Description Max. speed Max. (rpm) gravitational field (x g) 13450 Round bucket, sealable with cap no. 17170, for round adapters Ø 100 mm, (no. 17649 - 17699), for 650 ml tube no. 13456, adapter no. 13654, max.

  • Page 73: Maximum Speed For Tubes

    Refrigerated Centrifuge Sigma 4-16KS 11 Appendix Pos: 212 /10 0 Sigm a/11 0 BA Z entrif uge n Sigm a (Pr ojekt e)/4 -16KS_ 4-1 6KHS/110 A nhan g11 0-0 010 -00 10 H öchst dre hzahle n vo n Ge fäß en 4-1 6S_KS_KHS @ 29\ mo d_14 053 270 085 50_ 68.d ocx @ 198 849 @ 3 @ 1 11.1.1 Maximum speed for tubes...

  • Page 74: Speed-Gravitational-Field-Diagram

    Refrigerated Centrifuge Sigma 4-16KS 11 Appendix Pos: 216 /10 0 Sigm a/10 0 BA Z entrif uge n Sigm a (Sta nda rd mod ule)/ 110 A nha ng11 0-0 020 Dr ehza hl-Schwe ref eld-Di agr amm @ 2 8\m od_ 140 5320 705 642 _68. docx @ 19 515 3 @ 2 @ 1 11.2...

  • Page 75: Acceleration And Deceleration Curves

    Refrigerated Centrifuge Sigma 4-16KS 11 Appendix Pos: 218 /10 0 Sigm a/10 0 BA Z entrif uge n Sigm a (Sta nda rd mod ule)/ 110 A nha ng11 0-0 031 Beschl euni gun gs- und Br emsk urv en Spinc ont rol S @ 28\ mod _140 532 070 883 4_6 8.doc x @ 1 951 81 @ 2 @ 1 11.3...
  • Page 76 Refrigerated Centrifuge Sigma 4-16KS 11 Appendix Linear Curves 98 7 6 5 4 1000 curve 0 curve 1 curve 2 curve 3 curve 4 curve 5 curve 6 curve 7 curve 8 curve 9 Time [sec] Fig. 36: Diagram of linear curves...

  • Page 77: Table Of The Service Life Of Rotors And Accessories

    Refrigerated Centrifuge Sigma 4-16KS 11 Appendix Pos: 220 /10 0 Sigm a/10 0 BA Z entrif uge n Sigm a (Sta nda rd mod ule)/ 110 A nha ng11 0-0 040 T abell e: L eben sda uer v on R otor en und Zu behö r @ 28\ mod _14 053 2070 991 1_6 8.do cx @ 1 951 95 @ 2 @ 1 11.4...
  • Page 78 Refrigerated Centrifuge Sigma 4-16KS 11 Appendix Pos: 222 /10 0 Sigm a/10 0 BA Z entrif uge n Sigm a (Sta nda rd mod ule)/ 110 A nha ng11 0-0 050 Best ändig keitsta belle @ 28 \mo d_1 405 320 711 439_ 68. docx @ 19 520 9 @ 2 @ 1 Version 07/2012, Rev.

  • Page 79: Resistance Data

    Refrigerated Centrifuge Sigma 4-16KS 11 Appendix 11.5 Resistance data The data refer to resistance at 20°C. NOTE - no data 1 resistant 2 practically resistant 3 partially resistant 4 not resistant Medium Formula Acetaldehyde Acetamide saturated Acetone Acrylonitrile Allyl alcohol...
  • Page 80 Refrigerated Centrifuge Sigma 4-16KS 11 Appendix - no data 1 resistant 2 practically resistant 3 partially resistant 4 not resistant Medium Formula Chromic acid Chromic potassium KCr(SO saturated sulphate Citric acid Citric acid Copper sulphate CuSO x 5H Cyclohexanol Decane...
  • Page 81 Refrigerated Centrifuge Sigma 4-16KS 11 Appendix - no data 1 resistant 2 practically resistant 3 partially resistant 4 not resistant Medium Formula Isopropyl alcohol Lactic acid Magnesium chloride MgCl Mercuric chloride HgCl Mercury Methyl acetate Methyl alcohol Methyl benzene Methyl ethyl ketone...
  • Page 82 Refrigerated Centrifuge Sigma 4-16KS 11 Appendix - no data 1 resistant 2 practically resistant 3 partially resistant 4 not resistant Medium Formula Sodium bisulphite NaHSO Sodium carbonate Sodium chloride NaCl Sodium hydroxide NaOH Sodium hydroxide NaOH Sodium sulfate Spirits Styrene...

  • Page 83: Ec Declaration Of Conformity

    Refrigerated Centrifuge Sigma 4-16KS 11 Appendix Pos: 224 /10 0 Sigm a/11 0 BA Z entrif uge n Sigm a (Pr ojekt e)/4 -16KS_ 4-1 6KHS/110 A nhan g11 0-0 060 Konfo rmit ätse rklär ung 4- 16KS_KHS @ 29 \mo d_1 405 327 009 359_ 68. docx @ 19 8863 @ 2 @ 1 11.6...
  • Page 84 Refrigerated Centrifuge Sigma 4-16KS 11 Appendix === E nde der Liste für Tex tma rke I nhal t = == Version 07/2012, Rev. 1.11 of 06/11/2015 • sb Translation of the original operating manual, part no. 07057...

  • Page 85: Index

    Refrigerated Centrifuge Sigma 4-16KS Index 12 Index Centrifugation with low capacity ....30 Centrifuge cannot be started ...... 55 Acceleration ..........37 Centrifuge decelerates during operation ..55 Acceleration curve ......37, 48, 75 Centrifuge is inclined ........55 Acceleration curve (changing) ....48 Centrifuge was moved during run ....
  • Page 86 Refrigerated Centrifuge Sigma 4-16KS Index Deactivating the help function ....49 Deceleration (brake) ........37 General conditions ........9 Deceleration curve ......37, 48, 75 Glass breakage .......... 62 Declaration of conformity ..... 10, 83 Glass particles ........... 62 Declaration of decontamination ....65 Gravitational field ........
  • Page 87 Refrigerated Centrifuge Sigma 4-16KS Index Lid cannot be opened ........ 55 Lid error ............. 57 Online download of forms ......66 Lid lock device ........... 22 Open lid after run ........45 Lid lock has not released ......55 Opening the lid ........... 27 Lid seal sticks ..........
  • Page 88 Refrigerated Centrifuge Sigma 4-16KS Index Remove glass particles and metal dust from Slushing oil ..........10 the rotor chamber ........62 Solvents ......... 20, 59, 61 Responsibility of the operator ..... 17 Sound signal ..........22 Return of centrifuges, spare parts, or Sound signal (warning) ......
  • Page 89 Year of manufacture ........12 Useful volume - volume that is stated for the tube ..31, 73 Донау Лаб. Москва/ «Donau Lab. Moscow» - официальный дистрибьютер оборудования Sigma www.donaulab.ru Тел. +7 (495)-255-33-89 Адрес: 119034, Москва, Турчанинов пер, д.6, стр.2 Sigma Посмотреть...

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