SCIEX X500 QTOF Mass Spectrometer Manuals

Manuals and User Guides for SCIEX X500 QTOF Mass Spectrometer. We have 2 SCIEX X500 QTOF Mass Spectrometer manuals available for free PDF download: System User's Manual

SCIEX X500 QTOF System User's Manual (234 pages)

System

Brand: SCIEX | Category: Laboratory Equipment | Size: 5.04 MB

Table of Contents
3
Chapter 1 Operational Precautions and Limitations

8
- General Safety Information
  8
- Regulatory Compliance
  8
  - Australia and New Zealand
    8
  - Canada
    9
  - Europe
    9
  - United States
    9
  - International
    10
- Electrical Precautions
  10
  - AC Mains Supply
    10
  - Protective Earth Conductor
    11
- Chemical Precautions
  11
  - System Safe Fluids
    12
- Ventilation Precautions
  13
- Environmental Precautions
  14
  - Electromagnetic Environment
    15
  - Decommissioning and Disposal
    15
- Equipment Use and Modification
  16
- Qualified Personnel
  16
- Contact Us
  17
- Technical Support
  17
- Documentation Symbols and Conventions
  17
Chapter 2 Principles of Operation

19
- System Overview
  19
- Hardware Overview
  20
  - Panel Symbols
    24
- Theory of Operation
  24
  - Data Handling
    25
- Theory of Operation-SCIEX os
  25
  - Software Overview
    25
  - Scan Techniques
    25
  - Quantitative Analysis
    28
  - Integration
    28
  - Results Tables
    28
  - Calibration Curves
    28
  - Regression Equations
    29
  - Weighting Factors
    30
  - Regression Types
    30
  - Qualitative Analysis
    33
Chapter 3 Operating Instructions Hardware

36
- Start up the System
  36
- Shut down and Vent the System
  37
- Diverter Valve
  38
  - Plumb the Diverter Valve in Injector Mode
    39
  - Plumb the Diverter Valve in Diverter Mode
    40
- Calibrant Delivery System
  41
  - Replace the CDS Bottle
    41
  - Start the CDS
    42
  - Stop the CDS
    42
  - Flush the CDS
    42
Chapter 4 Configure Devices

45
- Add Devices
  45
- Edit Device Settings
  45
- Delete Devices
  46
- Deactivate Devices
  46
Chapter 5 Configure Access to the Software

48
- Users Overview
  48
  - Roles and Permissions
    48
  - Access to Analytics Features
    50
  - Add Users
    53
  - Deactivate a User
    53
  - Remove a User
    54
- Enable Full Screen Mode
  54
- Select Laboratory Information Management System (LIMS) Settings
  54
- Select Queue Options
  54
- Select Regional Settings
  55
- Manage the Compound Libraries
  55
Chapter 6 Operating Instructions Software

66
- About the Home Page
  66
- About the Ribbon and Launcher
  67
- About the Status Panel
  69
  - Add a Project
    71
  - Select a Project
    72
  - Control the Device Status
    72
  - Show the Status Panel
    72
  - Hide the Status Panel
    72
- Data Acquisition Panel
  72
- User Workflows
  73
  - Analysts
    73
  - Method Developers
    74
  - Administrators
    74
  - Reviewers
    74
- Batch and Queue Workspaces
  74
- MS Method Workspace
  88
  - Create an MS Method
    88
  - MS Method Experiments
    90
  - About MS Methods
    91
  - MS Method Parameters
    93
  - Calculate the Dynamic Collision Energy for MS Methods
    103
- LC Method Workspace
  104
  - Create an LC Method
    104
- Explorer Workspace
  104
  - Verify the Presence of an Analyte
    104
  - Extract Ions
    105
  - Open a Total Ion Chromatogram
    108
  - Open a Base Peak Chromatogram
    110
  - Show the Data and Peaks Table
    112
  - Show Sample Information
    114
  - Show the Graph Selection Information
    115
  - Edit Settings in Graphs
    120
  - Work with Data in Graphs
    122
  - Use the Two-Pane Operation Tools
    128
  - Move Panes or Windows
    129
  - Perform a Gaussian Smooth
    131
  - Threshold Data
    132
  - Subset Data (to Graph Selection)
    134
  - Baseline Subtract Chromatogram
    135
  - Offset Chromatogram
    137
  - Centroid a Spectrum
    138
  - Export Data as Text
    140
  - Export the Peak List as Text
    142
  - Print Data
    142
  - Reset Options
    143
  - Set Options
    143
- Analytics Workspace
  147
  - Set Project Secure Export Settings
    147
  - Enable Project Modified Peak Warning
    148
  - Define the Project Default Settings
    148
  - Create a Processing Method
    148
  - About Results Tables
    150
  - Review Peaks
    169
  - About Statistics Pane
    176
  - Calibration Curve: Options
    179
  - Analyzing Data Using Metric Plots
    181
  - Audit Trails
    183
- Integration Algorithm Parameters
  186
  - MQ4 Integration Algorithm Parameters
    186
  - Autopeak Integration Algorithm Parameters
    188
- Edit Report Templates
  189
  - Reporter Templates
    191
- MS Tune
  192
  - Perform a Quick Status Check
    192
  - Optimize the Detector
    193
  - Tune Q1
    194
  - Tune TOF MS
    194
  - Tune Q1 High
    195
  - Perform Advanced Troubleshooting
    196
  - Restore Instrument Data
    196
- Event Log Workspace
  197
  - View Logs
    197
  - Print Logs
    197
  - Archive Logs
    197
Chapter 7 Service and Maintenance Information

199
- Recommended Maintenance Schedule
  199
- Clean the Surfaces
  201
- Clean the Front-End
  201
  - Symptoms of Contamination
    202
  - Required Materials
    202
  - Cleaning Best Practices
    203
  - Prepare the Mass Spectrometer
    205
  - Clean the Curtain Plate
    206
  - Clean the Front of the Orifice Plate
    207
  - Put the Mass Spectrometer Back in Service
    207
- Empty the Source Exhaust Drain Bottle
  207
- Replace the Check Valve and Flow Module
  210
- Inspect the Roughing Pump Oil Level
  211
- Storage and Handling
  212
- Move the Mass Spectrometer
  213
- Generate a Support Package
  219
Chapter 8 Mass Spectrometer Troubleshooting

220
Appendix A Recommended Calibration Ions

223
- APCI Calibration Ions
  223
- ESI Calibration Ions
  225
Appendix B Exact Masses and Chemical Formulas

228
Appendix C Glossary of Symbols

229
Appendix D Glossary of Warnings

233

SCIEX X500 QTOF System User's Manual (82 pages)

QTOF System

Brand: SCIEX | Category: Laboratory Equipment | Size: 1.85 MB

Table of Contents
3
Operational Precautions and Limitations
6
General Safety Information
6
Documentation Symbols and Conventions
6
Regulatory Compliance
7
Australia and New Zealand
7
Canada
7
Europe
7
United States
8
International
8
Electrical Precautions
9
Mains Supply
9
Protective Earth Conductor
9
Chemical Precautions
10
System Safe Fluids
11
Ventilation Precautions
12
Physical Precautions
13
Environmental Precautions
13
Electromagnetic Environment
14
Decommissioning and Disposal
15
Qualified Personnel
15
Laboratory Conditions
16
Safe Environmental Conditions
16
Performance Specifications
16
Equipment Use and Modification
17
Principles of Operation
18
System Overview
18
Hardware Overview
19
Theory of Operation
22
Operating Instructions - Hardware
23
Start up the System
23
Shut down and Vent the System
24
Diverter Valve
25
Plumb the Diverter Valve in Injector Mode
26
Plumb the Diverter Valve in Diverter Mode
27
Calibrant Delivery System
29
Replace the CDS Bottle
29
Start the CDS
29
Stop the CDS
30
Flush the CDS
30
Operating Instructions - User Workflows
34
Operating Instructions-Device Configuration
36
Add Devices
36
Deactivate Devices
37
Service and Maintenance Information
38
Recommended Maintenance Schedule
38
Clean the Surfaces
40
Clean the Front-End
41
Symptoms of Contamination
41
Required Materials
41
Cleaning Best Practices
42
Prepare the Mass Spectrometer
44
Clean the Curtain Plate
45
Clean the Front of the Orifice Plate
46
Put the Mass Spectrometer Back in Service
46
Empty the Source Exhaust Drain Bottle
47
Replace the Check Valve and Flow Module
49
Replace the CDS Bottle Intake Filters
50
Inspect the Roughing Pump Oil Level
51
Storage and Handling
52
Move the Mass Spectrometer
53
Open the Dress Panel
60
Mass Spectrometer Troubleshooting
61
A Recommended Calibration Ions
67
APCI Calibration Ions
67
ESI Calibration Ions
69
B Exact Masses and Chemical Formulas
71
C Glossary of Symbols
73

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More SCIEX Manuals

SCIEX X500 QTOF Mass Spectrometer Manuals

SCIEX X500 QTOF System User's Manual (234 pages)

Table of Contents

Chapter 1 Operational Precautions and Limitations

Chapter 2 Principles of Operation

Chapter 3 Operating Instructions Hardware

Chapter 4 Configure Devices

Chapter 5 Configure Access to the Software

Chapter 6 Operating Instructions Software

Chapter 7 Service and Maintenance Information

Chapter 8 Mass Spectrometer Troubleshooting

Appendix A Recommended Calibration Ions

Appendix B Exact Masses and Chemical Formulas

Appendix C Glossary of Symbols

Appendix D Glossary of Warnings

SCIEX X500 QTOF System User's Manual (82 pages)

Table of Contents

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