Agilent Technologies 5975 MSD Service Manual
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Agilent Technologies 5975 MSD Service Manual

Sim direct inlet probe
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Scientific Instruments Manufacturer GmbH
D-46149 Oberhausen •
+49-208-94 10 78-0 • www.sim-gmbh.de
SERVICE MANUAL
SIM Direct Inlet Probe
for
Agilent 5975 MSD
and
Agilent 7000 Triple Quadrupole
(Firmware V.1.10)
- 1 -

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Summary of Contents for Agilent Technologies 5975 MSD

  • Page 1 Scientific Instruments Manufacturer GmbH D-46149 Oberhausen • +49-208-94 10 78-0 • www.sim-gmbh.de SERVICE MANUAL SIM Direct Inlet Probe Agilent 5975 MSD Agilent 7000 Triple Quadrupole (Firmware V.1.10) - 1 -...
  • Page 2 Scientific Instruments Manufacturer GmbH D-46149 Oberhausen • +49-208-94 10 78-0 • www.sim-gmbh.de Document History Edition 7075e 10/2010, from Firmware / Software Version V1.10 and dip.v.1.2. The information contained in this document is subject to change without notice. SIM GmbH makes no warranty of any kind with regard to this material, including, but not limited to, the implied warranties of merchantability and fitness for a particular purpose.

  • Page 3: Table Of Contents

    DIP INSTALLATION PROCEDURE ................5 Replacing the ion source ................... 5 Installing the DIP on the Agilent 5975 MSD ............... 5 Installing the DIP on the Agilent 7000 Triple Q ............7 Connecting the DIP and the GC ................. 8 Configuration of the DIP-Controller ................

  • Page 4: Parameter Menu Of The Controller (Firmware V1.10)

    Scientific Instruments Manufacturer GmbH D-46149 Oberhausen • +49-208-94 10 78-0 • www.sim-gmbh.de 1 Parameter Menu of the Controller (Firmware V1.10) Parameter Assignment min value max value default 1000 (Password) 0x7fff 1000 Temp. adjustment (0.1° C) -200 LCD contrast push rod position outside (min pos) -400 -100 -136...

  • Page 5: Dip Installation Procedure

    (EI or CI). Installing the DIP on the Agilent 5975 MSD Before installing the DIP System to the Agilent 5975 MSD you have to uninstall the MSD front panel: 1. After you have...
  • Page 6 Scientific Instruments Manufacturer GmbH D-46149 Oberhausen • +49-208-94 10 78-0 • www.sim-gmbh.de 3. Remove the DIP front panel of the DIP System following the instructions given in the DIP manual (chapter 7.2). 4. Take the DIP front panel and mount the display boards of the MSD onto the preset positions (see left).

  • Page 7: Installing The Dip On The Agilent 7000 Triple Q

    Scientific Instruments Manufacturer GmbH D-46149 Oberhausen • +49-208-94 10 78-0 • www.sim-gmbh.de 10. Mount the push rod cover by reversing the instructions in chapter 7.2 of the DIP manual. Make sure that all cables are correctly connected. Installing the DIP on the Agilent 7000 Triple Q Before installing the DIP System to the Agilent 7000 Triple Q MS/MS you have to uninstall the MSD front panel.

  • Page 8: Connecting The Dip And The Gc

    Scientific Instruments Manufacturer GmbH D-46149 Oberhausen • +49-208-94 10 78-0 • www.sim-gmbh.de 6. Take the adapter plate and mount it in front of the ion source compartment using the four screws (see marked circles on the left, the two screws behind the motors are not visible on this photo).

  • Page 9: Configuration Of The Dip-Controller

    Scientific Instruments Manufacturer GmbH D-46149 Oberhausen • +49-208-94 10 78-0 • www.sim-gmbh.de connecting diagram GC-MS-DIP Controller Controller Start-Remote-Cable Diode Cable Remotemanager B 0301 40 02 B 0613 59 73 RM 0002 68 90 Configuration of the DIP-Controller The IP adress is assigned in the menu “Network configuration “ of the DIP controller (see MSD DIP Manual, 5.5 Network configuration): 1.

  • Page 10: Insert The Chemstation/Masshunter Methods For The Dip

    2.10 Tuning of the DIP-MS System 2.10.1 Autotune 5975 MSD with DIP 1. Verify that the system has been pumping down for at least 2-4 hours and that the DIP controller is turned on. The DIP push rod status is “Ready”.

  • Page 11: Autotune 7000 Tripleq Ms/Ms With Dip

    Scientific Instruments Manufacturer GmbH D-46149 Oberhausen • +49-208-94 10 78-0 • www.sim-gmbh.de 3. When the autotune has completed, save it as “ATUNE.U”, and then select Tune Evaluation from the Qualify menu. The software will evaluate the last autotune and print a System Verification – Tune report. 4.

  • Page 12: Exact Positioning Of The Push Rod In The Ion Source

    This chapter is valid for all DIP systems for the Agilent 7000 Triple Q and for those for the 5975 MSD starting from serial number SN1938 (December 2009) because these systems are not equipped with an inspection glass any longer: In case of maintenance work at the push rod or for installing purposes it can be necessary to reposition the push rod in the ion source.
  • Page 13 Scientific Instruments Manufacturer GmbH D-46149 Oberhausen • +49-208-94 10 78-0 • www.sim-gmbh.de Press the arrow keys to open the valve (control it by watching the marker of the valve plug which is directed forwards to the observer when the valve is open, see blue arrow in figure on the left).

  • Page 14: Temperature Calibration Of The Controller

    Scientific Instruments Manufacturer GmbH D-46149 Oberhausen • +49-208-94 10 78-0 • www.sim-gmbh.de 4 Temperature Calibration of the Controller Menu: General Configuration This menu is used to select the language (German or English). Moreover, it is possible to change the operational mode which is reserved to the service engineers! 1.
  • Page 15 Scientific Instruments Manufacturer GmbH D-46149 Oberhausen • +49-208-94 10 78-0 • www.sim-gmbh.de 8. Select parameter “11” in the parameter menu and enter the calculated value in the following manner: ”-80” and <Enter> (for the above mentioned example, if the value of the controller is higher than the actual value).

  • Page 16: Dip Test Procedures

    Scientific Instruments Manufacturer GmbH D-46149 Oberhausen • +49-208-94 10 78-0 • www.sim-gmbh.de 5 DIP Test Procedures Evaluates the DIP tip temperature using a probe DIP Temperature Accuracy Test with a calibrated thermometer. Air/Water Check during DIP operation Evaluates the DIP for leaks. Evaluates the function of the DIP (45°...

  • Page 17: Leak Test

    The leak test of DIP/MS-System is passed, when the results of both measurements do not essentially differ. REQUIREMENTS - an autotune and tune evalutation test (for 5975 MSD) or “Air And Water Check” (for 7000 Triple Q) have just been performed. CONDITIONS - MS –...

  • Page 18: Coupling Test: Combipal With Msd-Dip And Gc (Optional, For Dip - 45° Type With 5975 Msd)

    < 2 Ratio 28/69 Coupling test: CombiPAL with MSD-DIP and GC (optional, for DIP - 45° type with 5975 MSD) This procedure checks the function of the CombiPAL autosampler by alternating injections into the DIP system and the GC. REQUIREMENTS - Two additional DIP positions have been defined in the CycleComposer software according to the DIP manual.

  • Page 19: Dip (Ei) Performance Test

    “Total Runtime” which is displayed in the DIP software (DIP method “check_EI.dip”, see DIP manual). - Optional: CombiPAL is installed correctly on the GC/MSD-DIP system (see DIP manual) CONDITIONS for DIP/5975 MSD Ready / Bereit DIP method check_EI.dip (30° C for 0.1 min, 30-350° C at 0.5° /s, 350° C for 5 min)
  • Page 20 Sample volume 1 µl PROCEDURE Set up the Methods 1. Load method DIP_EI_Q1.M for the 5975 MSD (MS ChemStation) or DIP_EI_Scan.M for the 7000 Triple Q MS/MS. 2. Select the actual autotune using Instrument/Select MS Tune File (ATUNE.U or atunes.ei.tune.xml).
  • Page 21 Scientific Instruments Manufacturer GmbH D-46149 Oberhausen • +49-208-94 10 78-0 • www.sim-gmbh.de The following steps have to be performed with the push rod tip for liquid samples (A) and the tip for solid samples (B): 1. After loading the DIP method, click the Start button (green arrow) in the Instrument Control view (of the MS software) and specify all sample information in the Sample Information panel.

  • Page 22: Dip (Pci) Performance Test For Dip/5975 Msd Systems

    D-46149 Oberhausen • +49-208-94 10 78-0 • www.sim-gmbh.de DIP (PCI) Performance test for DIP/5975 MSD Systems This test uses a traceable standard solution to determine the correct performance of the DIP. Perform this procedure on both types of probe tips (for liquid and for solid samples).
  • Page 23 +49-208-94 10 78-0 • www.sim-gmbh.de PROCEDURE Set up the Methods 1. Load method DIP_CI_Q1.M for the 5975 MSD (MS ChemStation). 2. Select PCICH4.U using Instrument/Select MS Tune File. 3. Save the method to “…\1\METHODS\DIP_CI_Q1.M” 4. Print the method and verify that method and conditions are the same 5.

  • Page 24: Appendix

    Scientific Instruments Manufacturer GmbH D-46149 Oberhausen • +49-208-94 10 78-0 • www.sim-gmbh.de APPENDIX DIP-Methods drive.dip 30° C for 0.1 min, 30-35° C at 0.5° /s, 35° C for 0.05 min heat.dip 30° C for 0.1 min, 30-400° C at 2.0° /s, 400° C for 1 min a_w_check.dip 30°...

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7000 triple quadrupole

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