HP 5890 Series II Plus Reference Manual page 233

Test Sample Chromatograms
Test sample chromatograms
Figure 10-9.
Detector Type
Temp 300 DEGREES C
Inlet Type Split only or
split/splitless
Temp 250 DEG C
Operating Mode Split(Purge on)
Purge Time On
Purge Time Off
Oven Temp Programmed
Init Temp
Init Time
Ramp
Rate
Fin Temp
Fin Time
Range 0
COLUMN:
Part No. 19095Z(121)
Dimensions
Sta Phase Methyl Silicone
TCD-Split Mode Capillary Inlet
HP 5890 Test Sample Operating
Conditions
TCDw/MUG
0 min
0 min
100 DEGREES C
1 min
10
150
2
¿
530 MID; 5 M
START
FLOW RATES
Carrier (He) 15 +/• 1
Hydrogen
Air
Makeup (He) 10 +/• 1
Split Vent 200 +/• 10
Septum Purge 5 +/• 1
Reference (He)37 +/• 1
SAMPLE:
Type Capillary
¿
Inj Volume 1
Part No. 18740•60900
Composition See Split/FID
.11
.25
3.64
3.85
4.78
ST
ml/min
N/A ml/min
N/A4 ml/min
ml/min
ml/min
ml/min
ml/min
l
.15
C9
6.48
C16
.42
4.45
233