HP 5890 Series II Plus Reference Manual page 231

Test Sample Chromatograms
Test sample chromatograms
Figure 10-7.
Detector Type NPD w/MUG
Temp 220 DEGREES C
Inlet Type Split only or
split/splitless
Temp 200 DEGREES C
Operating Mode Split(Purge on)
Purge Time On
Purge Time Off
Oven Isothermal
Init Temp
Init Time
Ramp
Rate
Fin Temp
Fin Time
Range 0
COLUMN:
Part No.
Dimensions
Sta Phase
NPD-Split Mode Capillary Inlet
HP 5890 Test Sample Operating
Conditions
0 min
0 min
180 DEGREES C
5.0 min
0
19095Z(#121)
¿
530 MID; 10 M
START
3
2.
ST
FLOW RATES
Carrier (He)
Hydrogen
Air
Makeup (He)
Split Vent
Septum Purge
SAMPLE:
Type NP-FID Sample
Inj Volume
Part No. 18789•60060
Composition 0.65 ppm azobenzene,
100 ppm octadecane, 1.0 ppm
malathion in isooctane
3
1. 5
C18
7
3.22
15 +/• 1 ml/min
3.5 +/• 0.1 ml/min
100•120 +/• 10 ml/min
10+/•1 ml/min
80+/•5 ml/min
5+/•1 ml/min
¿
2 l
AZOBENZENE
MALATHION
231