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TRACE GC Ultra
Thermo Scientific TRACE GC Ultra Manuals
Manuals and User Guides for Thermo Scientific TRACE GC Ultra. We have
2
Thermo Scientific TRACE GC Ultra manuals available for free PDF download: Maintenance And Troubleshooting Manual, Installation Manual
Thermo Scientific TRACE GC Ultra Maintenance And Troubleshooting Manual (412 pages)
Brand:
Thermo Scientific
| Category:
Laboratory Equipment
| Size: 6.44 MB
Table of Contents
Table of Contents
5
About this Manual
11
Overview
11
Conventions Used in this Manual
13
Instrument Markings and Symbols
16
Using Hydrogen
17
Using the Hydrogen Sensor
18
Preventive Maintenance
21
Suggested Maintenance Schedule
22
Maintaining a Split/Splitless Injector
25
Split/Splitless Injector
26
Split/Splitless Injector Maintenance
28
When Cleaning or Replacing the Liner
28
When Replacing the Septum
28
If the Glass Liner Breaks Inside the Injector
29
When Replacing the Split Line Tubing
29
Maintaining a Large Volume Splitless Injector
53
Large Volume Splitless Injector
54
Large Volume Splitless Injector Maintenance
56
When Cleaning or Replacing the Liner
56
When Replacing the Septum
56
If the Glass Liner Breaks Inside the Injector
57
When Replacing the Split Line Tubing
57
Maintaining a Cold On-Column Injector for Standard Automatic Injections
79
Automated Operation Cold On-Column Injector
80
Cold On-Column Injector Maintenance
82
Possible Leaks in the Rotary Valve
82
Replace the O-Ring
82
Operating Sequences
83
Replace the O-Ring
83
Replace the Rotary Valve Seal
87
Maintaining a Cold On-Column Injector Direct Narrow-Bore
97
Automated Operation Cold On-Column Injector
98
Cold On-Column Injector Maintenance
100
Possible Leaks in the Rotary Valve
100
Maintaining a Cold On-Column Injector
111
Injector
112
Manual Cold On-Column
112
Manual Cold On-Column Injector
112
Cold On-Column Injector Maintenance
114
Possible Leaks in the Rotary Valve
114
Replace the Rotary Valve Seal
115
Maintaining a Packed Column Injector
121
Packed Column Injector
122
Packed Column Injector Maintenance
124
When Replacing the Septum
124
Maintaining a Purged Packed Column Injector
129
Purged Packed Column Injector
130
Purged Packed Column Injector Maintenance
132
When Replacing the Liner
132
When Replacing the Septum
132
Replace the Septum
133
Clean or Replace the Liner
136
Maintaining a Ptv Injector
141
PTV Injector
142
PTV Injector Maintenance
144
When Replacing the Septum
144
When Cleaning or Replacing the Liner
145
Adjusting the Quartz Wool Packing
146
If a Liner Breaks Inside the Injector
146
Replace the Septum
147
Clean or Replace the Liner
151
Replace a Broken Liner
157
Adjust a Quartz Wool Packing
165
Discrimination
171
Large Volume PTV
171
PTV Troubleshooting
171
Sensitivity
171
Troubleshooting the PTV Injector
172
Ensuring Tightness
179
Chapter 10 Ensuring Tightness
179
DCC-Equipped Systems
180
Keeping Leaks under Control
180
Leak Check
180
Performing a Leak Check (Capillary Column)
181
Performing a Leaks Check (Capillary/Packed/Ufm Columns)
185
Leak Test the Lines from the Gas Source to the GC
188
Multiple Systems
188
Maintaining a Fid
191
Chapter 11 Maintaining a FID
191
Flame Ionization Detector (FID)
192
FID Maintenance
194
Clean the Jet
195
Replace the Jet
199
Clean the Collecting Electrode
202
Replace the Collecting Electrode
207
Replace the Ignition Assembly
211
Change in Sensitivity
214
FID Troubleshooting
214
Gases
214
Flame Ignition
215
Contamination
217
Maintaining an Electron Capture Detector
219
Electron Capture Detector (ECD)
220
ECD Maintenance
222
Wipe Test
223
Wipe Test Certificate
224
Clean the Collecting Electrode
226
Replace the Collecting Electrode
229
Replace the Silver Seal
232
Change in Sensitivity
235
ECD Troubleshooting
235
Gases
235
Temperature
235
Contamination
236
Troubleshooting the ECD
237
Maintaining a Nitrogen Phosphorus Detector
239
Nitrogen Phosphorus Detector (NPD)
240
NPD Maintenance
242
Thermionic Source
242
Clean the Jet
243
Replace the Jet
247
Clean the Collecting Electrode
251
Replace the Collecting Electrode
256
Replace the NPD Thermionic Source
260
Gases
264
NPD Troubleshooting
264
Sensitivity
264
Troubleshooting the NPD
266
Maintaining a Flame Photometric Detector
269
Flame Photometric Detector (FPD)
270
FPD Maintenance
272
Clean the Jet
273
Clean the Interferential Filter
278
Clean the Mirror Metal Plug
282
Clean the Flame-Side Heat Shield
287
Replace the Jet
292
Replace the Interferential Filter
297
Replace the Heat Shields
301
FPD Troubleshooting
310
Gases
310
Sensitivity
310
Troubleshooting the FPD
312
Maintaining a Photoionization Detector
315
Photoionization Detector (PID)
316
Leaks
318
PID Maintenance
318
Contamination
334
Lamp
334
PID Troubleshooting
334
Sensitivity
334
Troubleshooting the PID
335
Maintaining a Thermal Conductivity Detector
337
Thermal Conductivity Detector (TCD)
338
TCD Maintenance
340
Baseline Drift
341
Negative Peaks
341
Sensitivity
341
TCD Troubleshooting
341
Troubleshooting the TCD
342
Maintaining Detectors in Stack Configuration
345
ECD Adapted for Stack Configuration
346
Guidelines for Maintenance
348
Clean or Replace the Collecting Electrode
349
Ecd)
349
Clean or Replace the Collecting Electrode (NPD on ECD)
356
Clean or Replace the Collecting Electrode
363
Ecd)
363
Ecd)
369
Replace the Silver Seal
369
Replace the Silver Seal (NPD on ECD)
375
Ecd)
381
Replace the Silver Seal
381
Incorrect Installation of the Column
386
Troubleshooting Guidelines
386
Regenerating Carrier and Split Lines Filters
387
Analytical Troubleshooting
391
Customer Communication
401
How to Contact Us
401
Reader Survey
402
Acetone
403
Reagents Safety Information
403
Methanol
404
Toluene
404
Glossary
405
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Thermo Scientific TRACE GC Ultra Installation Manual (28 pages)
Brand:
Thermo Scientific
| Category:
Laboratory Equipment
| Size: 1.14 MB
Table of Contents
Table of Contents
3
Nitrogen Phosphorus Detector
5
About this Guide
6
Introduction
6
Who Performs the Installation of the Kit
6
Detector Gases Requirements
6
Phosphorus Detector on Your TRACE GC Ultra
6
Transformer for NPD
7
Getting Started
7
Removing the GC Panels
9
Operating Sequences Installing NPD Upgrade Kit
9
Figures the TRACE GC Ultra
9
TRACE GC Ultra Top Cover
10
TRACE GC Ultra Rear Panel
11
GC Rear Panel Fixing Screws
12
Installing the NPD Control Card
13
Extension Slots Top View
13
Detector Control Card Expansion Slots
14
Removing the Power Control Module
16
TRACE GC Ultra Right Side View
16
TRACE GC Ultra Rear View
17
Install the Transformer for Detector
18
Transformer Installation
18
Transformer Assembly Identification Parts
19
Reinstall the Power Control Module
20
Installation of the Transformer for NPD
20
Mounting the NPD on the GC
21
Jet for NPD
21
Reinstall the GC Panels
22
Restarting the GC
23
Configuration
24
Hardware Configuration
24
Detector and Make-Up Gas Configuration
24
Configuring Hardware, Detector and Make-Up Gas
24
Set NPD Parameters
26
Parameters Setting
26
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