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Dionex ICS-1100
Thermo Scientific Dionex ICS-1100 Manuals
Manuals and User Guides for Thermo Scientific Dionex ICS-1100. We have
3
Thermo Scientific Dionex ICS-1100 manuals available for free PDF download: Operator's Manual, Manual, Preventive Maintenance Procedure
Thermo Scientific Dionex ICS-1100 Operator's Manual (168 pages)
Brand:
Thermo Scientific
| Category:
Laboratory Equipment
| Size: 1.69 MB
Table of Contents
Table of Contents
3
1 Introduction
11
Introduction to Ion Chromatography (IC)
11
Overview of the Dionex ICS-1100
14
About this Manual
15
Safety Messages and Notes
16
Safety and Regulatory Information
18
Safety Labels
18
2 Features
21
Operating Features
21
Front Panel
21
Top Cover
23
Component Panel
24
Right-Side Panel
27
Rear Panel
28
Flow Schematics
30
Chromeleon and Chromeleon Xpress
34
The Panel Tabset
34
Software Control Modes
35
System Wellness
35
System Component Details
36
Vacuum Degas Assembly (Optional)
36
Eluent Valve
38
Pump
38
Injection Valve
40
Auxiliary Valve (Optional)
42
Column Heater (Optional)
43
Suppressor
44
DS6 Heated Conductivity Cell
44
ER Controller
45
3 Operation and Maintenance
47
Operation Overview
47
Turning on the System Power
49
Connecting to Chromeleon
50
Set up the Eluent Reservoir
52
Prepare the Eluent
52
Degas the Eluent
52
Filter the Eluent
53
Fill the Reservoir
53
Set the Eluent Level
53
Connect the Reservoir
54
Check All Connections
54
Prime the Pump
55
Set System Operating Conditions
56
Equilibrate the System and Verify Operational Status
56
Prepare Samples
57
Collecting and Storing Samples
57
Pretreating Samples
58
Diluting Samples
58
Loading and Injecting Samples
59
Loading Samples with a Syringe
60
Loading Samples with a Vacuum Syringe
61
Loading Samples with an Autosampler
61
Injecting Samples
62
Processing Samples
62
Manual Sample Processing
62
Automatic (Batch) Sample Processing
63
Maintenance
65
4 Troubleshooting
69
Error Messages
69
Troubleshooting Error Messages
71
Liquid Leaks
78
Pump Difficult to Prime or Loses Prime
80
Pump Does Not Start
82
No Flow
82
Erratic Flow/Pressure Reading
83
Excessive System Backpressure
83
Peak "Ghosting
84
Nonreproducible Peak Height or Retention Time
85
Abnormal Retention Time or Selectivity
85
No Cell Response
86
High Cell Output
86
Baseline Noise or Drift
88
Vacuum Degas Assembly Does Not Run
89
5 Service
91
Diagnostic and Calibration Procedures
91
Chromeleon Wellness Panel Overview
92
Calibrating the Conductivity Cell
94
Calibrating the Flow Rate
96
Calibrating the Vacuum Degas Assembly
97
Isolating a Restriction in the Liquid Lines
97
Replacing Tubing and Fittings
100
Rebuilding the Injection Valve or Auxiliary Valve
101
Replacing an Auxiliary Valve Pod
102
Cleaning and Replacing the Pump Check Valves
105
Replacing a Pump Piston Seal and Piston Rinse Seal
107
Replacing a Pump Piston
111
Replacing the Waste Valve or Priming Valve O-Ring
112
Replacing the Conductivity Cell
114
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Thermo Scientific Dionex ICS-1100 Manual (16 pages)
Preventive Maintenance Procedure for Ion Chromatography Systems
Brand:
Thermo Scientific
| Category:
Laboratory Equipment
| Size: 0.2 MB
Thermo Scientific Dionex ICS-1100 Preventive Maintenance Procedure (12 pages)
Brand:
Thermo Scientific
| Category:
Laboratory Equipment
| Size: 1.55 MB
Table of Contents
Preventive Maintenance Procedure
3
Included Parts
3
Additional Items Required
4
Completing the Procedure
12
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