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DISCOVERY DSC250
TA DISCOVERY DSC250 Manuals
Manuals and User Guides for TA DISCOVERY DSC250. We have
1
TA DISCOVERY DSC250 manual available for free PDF download: Getting Started Manual
TA DISCOVERY DSC250 Getting Started Manual (61 pages)
DIFFERENTIAL SCANNING CALORIMETER
Brand:
TA
| Category:
Laboratory Equipment
| Size: 1.56 MB
Table of Contents
Introduction
3
Important: TA Instruments Manual Supplement
3
Notes, Cautions, and Warnings
4
Regulatory Compliance
4
Safety Standards
4
Electromagnetic Compatibility Standards
5
Safety
6
Instrument Symbols
6
Electrical Safety
7
Handling Liquid Nitrogen
7
Thermal Safety
8
Chemical Safety
8
Laser Safety
9
Lifting the Instrument
9
Table of Contents
10
Introducing the Discovery DSC™ 2500, DSC250, DSC25
12
Overview
12
DSC System Components
13
Discovery DSC
13
Discovery DSC Cell
13
Gas Delivery Module
15
DSC Autosampler
15
Cooling Accessories
15
Finned Air Cooling System (FACS)
16
Quench Cooling Accessory (QCA) for FACS
16
Stand-Alone Quench Cooler
16
Refrigerated Cooling System (RCS)
17
Liquid Nitrogen Pump (LN Pump)
18
The Discovery DSC™ User Interface
19
Primary Function Buttons
20
View Panel
21
Additional Function Buttons
22
Instrument Specifications
23
Options and Accessories
25
Tzero® Sample Encapsulating Press
25
Installing the Discovery DSC™ System
26
Unpacking/Repacking the DSC
26
Inspecting the System
27
Choosing a Location
27
Near
27
Away from
27
Setting up System Communication
30
Connecting Lines to the Gas Delivery Module
30
Purge Gas Lines
30
Cooling Gas Line
31
Connecting the Power Cable
32
Starting the Discovery DSC System
32
Shutting down the Discovery DSC System
33
Installing the DSC Cooling Accessories
34
Installing the Finned Air Cooling System (FACS)
34
Installing the Refrigerated Cooling System (RCS)
36
Installing the Quench Coolers
39
Quench Cool Accessory for FACS
39
Stand-Alone Quench Cooler
39
Installing the Liquid Nitrogen Pump (LN Pump)
40
Installing the Transfer Line
41
Installing the LN Pump to the Tank
43
Installing the LN Pump on the Discovery DSC
44
Installation of Additional Items
50
Installing the Autosampler Tray
50
Installing the Lid (DSC2500 Only)
50
Use, Maintenance, & Diagnostics
52
Using the Discovery DSC
52
Before You Begin
52
Calibrating the Discovery DSC
53
T1 Baseline Calibration (Discovery DSC2500, DSC250, DSC25)
53
Tzero ® Calibration
53
Enthalpy (Cell) Constant Calibration
54
Temperature Calibration
54
Heat Capacity Calibration (Discovery DSC2500 Only)
54
Heat Capacity (MDSC ® ) Calibration
54
Autosampler Calibration
55
Running a Discovery DSC™ Experiment
55
Experimental Procedure
55
Loading the Sample
55
Starting an Experiment
56
Stopping an Experiment
56
Maintaining the Instrument
56
Cleaning the User Interface Screen
56
Replacing Fuses
57
Replacement Parts
58
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