Micromeritics ASAP 2020 Confirm Manuals

Manuals and User Guides for Micromeritics ASAP 2020 Confirm. We have 1 Micromeritics ASAP 2020 Confirm manual available for free PDF download: Operator's Manual

Micromeritics ASAP 2020 Confirm Operator's Manual (436 pages)

Developer/Analyst

Brand: Micromeritics | Category: Measuring Instruments | Size: 9.85 MB

Table of Contents
5
General Information
13
Organization of the Operator's Manual
13
Conventions
14
Equipment Description
15
Gas Requirements
16
Analysis Program
16
Report System
16
Specifications
17
User Interface
21
Controls, Indicators, and Connectors
21
Front Panel
22
Side Panel
25
Upper
25
Lower
26
Rear Panel
27
Using the Software
28
Logging in
28
Shortcut Menus
28
Shortcut Keys
29
Dialog Boxes
30
Selecting Files
32
Menu Structure
34
Windows Menu
35
Help Menu
35
Operational Procedures
37
Creating File Templates
37
Creating Parameter Files
39
Sample Tube
39
Degas Conditions
40
Analysis Conditions
41
Adsorptive Properties
43
Report Options
44
Creating a Sample File
46
Analyst
46
Developer
48
Preparing Samples
50
Choosing Sample Tubes
50
Cleaning and Labeling Sample Tubes
51
Determining Amount of Sample to Use
55
Determining the Mass of the Sample
55
Degassing the Sample
57
Transferring the Degassed Sample to the Analysis Port
59
Installing Dewars
61
Precautions
61
Cold Trap Dewar
62
Analysis Dewar
63
Performing an Analysis
64
Printing File Contents
66
Listing File Statistics
67
Importing Sample and Parameter Files
68
Exporting a Sample Information File
69
Generating Graph Overlays
70
Multiple Samples Overlay
71
Multiple Graphs Overlay
74
File Menu
77
Description
77
New
79
Sample Information
79
Analyst
80
Developer
83
Sample Tube
88
Degas Conditions
90
Analysis Conditions
93
Adsorptive Properties
106
Report Options
110
Summary Report
114
Isotherm Report Options
116
Bet/Langmuir Surface Area Report Options
119
Freundlich Isotherm
122
Temkin Isotherm
124
T-Plot Report Options
126
Alpha-S Plot
133
F-Ratio Plot
135
BJH Adsorption/Desorption Report Options
137
Dollimore-Heal Adsorption/Desorption Report Options
145
Horvath-Kawazoe Report Options
146
DFT Pore Size
152
DFT Surface Energy
155
Dubinin Report Options
156
MP-Method Report Options
161
Options Report
165
Sample Log Report
165
Validation Report
166
Collected/Entered Data
167
Open
169
Sample Information File
169
Analyst
171
Developer
172
Templates
172
Parameter Files
173
Save
174
Save as
174
Save as Template
176
Save All
176
Close
177
Close All
177
Print
178
List
180
Import
181
Export
182
Format of Data Output
183
Convert
184
Log in
185
Log out
185
Exit
186
Unit Menu
187
Description
187
Sample Analysis
189
Start Degas
194
Enable Manual Control
195
Show Instrument Schematic
198
Show Status
199
Show Instrument Log
200
Unit Configuration
202
Diagnostics
204
Calibration
207
Vacuum Gauge
207
Pressure Zero
207
Pressure Scale
208
Temperature
208
Volume
209
Save to File
211
Load from File
211
Degas
212
Enable Manual Control
212
Show Instrument Schematic
213
Show Status
214
Calibrate Pressure Zero
215
Calibrate Pressure Scale
215
Calibrate Vacuum Gauge
216
Calibrate Servo
216
Service Test
217
Reports Menu
219
Description
219
Start Report
221
Close Reports
224
Open Report
224
SPC Report Options
225
Regression Report
226
Control Chart
230
Heat of Adsorption
233
Rate of Adsorption (ROA)
236
Printed Reports
237
Header
237
Onscreen Reports
237
Tool Bar
238
Shortcut Menus
242
Tabular Reports
242
Graphs
243
Zoom Feature
245
Axis Cross Hair
246
Report Examples
246
Tabular Report
247
Isotherm Plot
248
T-Plot
249
BET Surface Area Plot
250
BJH Adsorption
251
Summary Report
252
Options Report
253
Sample Log Report
254
Options Menu
255
Description
255
Add Archive Location
256
Edit Labels
257
Update File List
258
Units
258
Graph Grid Lines
259
Live Graph
260
Service Test Mode
260
Troubleshooting and Maintenance
261
Troubleshooting
261
Preventive Maintenance
263
Lubricating the Elevator Screw
265
Checking the Analysis Port Dewar
265
Replacing the Sample Tube O-Ring
266
Replacing the Port Filters
267
Analysis Port
267
Degas Port
268
Replacing the Vacuum Pump Exhaust Filter
268
Inspecting and Changing Vacuum Pump Fluid
269
Inspecting Fluid
269
Changing Fluid
269
Replacing the Alumina in the Oil Vapor Traps
272
Cleaning the Cold Trap Tubes
275
Calibrating the Manifold Temperature Sensor
276
Performing a Leak Test
277
Routine Maintenance
280
Cleaning the Analyzer
280
Calibrating the Pressure Offset
280
Calibrating the Pressure Scale
281
Cleaning and Verifying the Gas Line
282
Ordering Information
285
Analysis System Components and Accessories
285
Sample Tubes and Components
288
1/4-In., 3/8-In, and 1/2-In Sample Tubes
288
22-MM Sample Tube Kit
289
Cold Trap Tubes and Components
290
Forms
291
ASAP Series Sample Data Worksheet
293
Error Messages
295
2200 And 2300 Series
295
2400 Series
300
2500 Series
311
4000 Series
319
6200 Series
337
6500 Series
341
Calculations
353
Saturation Pressure (Po
353
Relative Pressure
353
Free Space
355
Equations of State
356
Quantity Adsorbed
357
Equilibration
358
Thermal Transpiration Correction
359
BET Surface Area
360
Langmuir Surface Area
361
T-Plot
363
BJH Pore Volume and Area Distribution
365
Explanation of Terms
365
Calculations
366
Compendium of Variables
373
Horvath-Kawazoe
374
Slit Pore Geometry (Original HK
374
Cylinder Pore Geometry (Saito/Foley
375
Sphere Pore Geometry (Cheng/Yang
376
Interaction Parameter
378
Additional Calculations
379
Interaction Parameter Components
380
Dubinin-Radushkevich
382
Dubinin-Astakhov
384
MP-Method
388
Freundlich Isotherm
390
Temkin Isotherm
391
DFT (Density Functional Theory
392
The Integral Equation of Adsorption
392
Application to Surface Energy Distribution
393
Application to Pore Size Distribution
393
Performing the Deconvolution
394
Regularization
394
Heat of Adsorption
395
Summary Report
395
SPC Report Variables
397
Regressions Chart Variables
397
Control Chart Variables
398
Testing for Leaks
399
Testing Individual Valves
399
Analysis Valves
399
Valves 3 and P1 through P6
402
Valves PS, 5, and 7
402
Valves 1, 2, 8, 9, 10, 11, and PV
403
Degas Valves
405
What to Do if You Detect a Leaking Valve
406
Removing Differential Pressure from a Leaking Valve
406
Repairing or Replacing a Leaking Valve
406
Repairing Valves on the Analysis Manifold
406
Replacing Valves on the Degas and Gas Inlet Manifold
408
Valve Data Test Sheet
409
Calculating Free-Space Values for Micropore Analyses
411
Dft Models
413
Models Based on Statistical Thermodynamics
413
Theoretical Background
413
Molecular Simulation Methods
414
Molecular Dynamics Method
414
Monte Carlo Method
414
Density Functional Formulation
415
Models Included
419
Non-Local Density Functional Theory with Density-Independent Weights
419
Non-Local Density Functional Theory with Density-Dependent Weights
419
Models Based on Classical Theories
425
Surface Energy
425
Pore Size
425
Models Included
426
Kelvin Equation with Halsey Thickness Curve
426
Kelvin Equation with Harkins and Jura Thickness Curve
426
Kelvin Equation with Broekhoff-De Boer Thickness Curve
427
References
427

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Micromeritics ASAP 2020 Confirm Operator's Manual (436 pages)

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