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JSM-6390 LA
JEOL JSM-6390 LA Manuals
Manuals and User Guides for JEOL JSM-6390 LA. We have
1
JEOL JSM-6390 LA manual available for free PDF download: User Manual
JEOL JSM-6390 LA User Manual (68 pages)
Scanning Electron Microscope
Brand:
JEOL
| Category:
Microscope
| Size: 62.27 MB
Table of Contents
Table of Contents
3
A) Generalities about the JEOL SEM @ IGP
5
A.1) Lab Overview
5
A.2) Computers
6
A.3) First Things to Do When You Arrive
6
A.4) Overview of the JEOL Console
7
A.5) Overview of the "JEOL Scanning Electron Microscope" Program
8
B) Starting Your Session
11
C) Sample Loading or Unloading
13
C.1) Opening the Sample Chamber
13
C.2) Removing/Loading a Sample & Closing the Chamber
13
D) Stage Motion
17
D.1) Horizontal Displacement (X, Y)
17
D.2) Vertical Displacement (Z)
17
D.3) Rotation (R)
17
D.4) Tilting (T)
17
E) Activate the Electron Beam
19
E.1) Activating a Lab 6 Electron Source in "Lab 6 Mode
19
E.2) Activating a W Electron Source in "Lab 6 Mode
19
F) Beam Alignment
21
F.1) Tilt & Shift Optimisation
21
F.2) Beam Alignment for Quantitative Analysis or SE/BSE Imaging
21
F.3) Beam Alignment for CL Imaging
22
G) Using the Cathodoluminescence (CL) Detector
27
G.1) Inserting or Removing the CL Detector
27
G.2) Activating the CL Detector
28
G.3) Deactivating the CL Detector
28
H) Thermo NSS Program
29
H.1) Starting "Thermo NSS
29
H.2) Overview of NSS and the Different Analysis Modes
31
I) SE, BSE, or CL Imaging with Thermo NSS
33
I.1) SE, BSE, or CL Imaging
33
I.2) SE, BSE, or CL Mosaic Imaging
35
I.3) Tips on Image Acquisition Time & Magnification
37
I.4) Exporting Your Images
37
J) Quantitative (or Qualitative) EDS Analysis
39
J.1) Load Standard Data
39
J.2) Single Spectrum
42
J.3) Point & Shoot
44
J.4) EDS Data (Re)Processing
46
J.4.1) Options for Analysis Processing
46
J.4.2) Reprocessing Data
46
J.4.3) Navigating in the Spectrum Panel
46
J.5) Exporting Quantitative EDS Data
47
J.5.1) Choice of Data to Export
47
J.5.2) Exporting a Single Spectrum
47
J.5.3) Exporting a Point & Shoot Analysis
47
K) EDS Element Mapping
49
K.1) Acquiring an Element Map with the Mode "Spectral Imaging
49
K.2) Treating Element or Phase Maps
51
K.2.1) Extracting "Element Maps
51
K.2.2) Extracting "Phase Maps
51
K.2.3) Extracting and Quantifying a "Spectrum" from of an Element Map
51
K.3) Additional Tips on Map Treatment after Extraction
54
Appendix
55
A1) Adjusting the SNS (Sample Navigation System)
55
A2) Activating the SEM in W-Mode
56
A3) Characteristic X-Ray
58
A4) Image Resolution
59
A5) EDS Mapping Time & Element Map Quality
60
A6) Thermo NSS Toolbars (from the NSS Manual)
62
A7) File Handling in Thermo NSS
63
A8) "Ispectra" by Christian Liebske
64
A9) Troubleshooting for Bad Analysis & Other Known Problems
65
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