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1260 Infinity G1315C
Agilent Technologies 1260 Infinity G1315C Manuals
Manuals and User Guides for Agilent Technologies 1260 Infinity G1315C. We have
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Agilent Technologies 1260 Infinity G1315C manual available for free PDF download: User Manual
Agilent Technologies 1260 Infinity G1315C User Manual (314 pages)
Diode Array and Multiple Wavelength Detector
Brand:
Agilent Technologies
| Category:
Laboratory Equipment
| Size: 6.58 MB
Table of Contents
Table of Contents
5
1 Introduction
9
Introduction to the Detector
10
Optical System
11
System Overview
14
Leak and Waste Handling
14
Bio-Inert Materials
16
2 Site Requirements and Specifications
19
Site Requirements
20
Physical Specifications
23
Performance Specifications
24
Specifications
24
Specification Conditions
36
3 Installing the Module
37
Unpacking the Detector
38
Damaged Packaging
38
Delivery Checklist
39
Optimizing the Stack Configuration
40
Two Stack Configuration
42
Installation Information on Leak and Waste Handling
44
Installing the Detector
48
Flow Connections to the Detector
51
Installing Capillaries
54
Setting up the LAN Access
60
4 Using the Detector
61
Leak and Waste Handling
62
Setting up an Analysis
63
Before Using the System
63
Requirements and Conditions
65
Optimization of the System
67
Preparing the HPLC System
68
Running the Sample and Verifying the Results
77
Special Settings of the Detector
78
Control Settings
78
Configuration Settings
79
Online Spectra (DAD Only)
80
Run Recovery Settings
81
Automated Run Recovery in Case of Temporary Communication Failures
82
Manual Run Recovery in Case of Permanent Communication Failures
84
Analog Output Settings
85
Spectrum Settings (DAD Only)
86
Peakwidth Settings
88
Slit Settings
90
Margin for Negative Absorbance Settings
91
Optimizing the Detector
91
Special Setups with Multiple DAD-Mwds
92
Two Detectors of same Type (E.g. G1315C/D and G1315C/D)
92
Two Detectors of Similar Type (E.g. G1315C/D and G1315A/B)
92
Solvent Information
93
5 How to Optimize the Detector
99
Introduction
100
Optimization Overview
101
Optimizing for Sensitivity, Selectivity, Linearity and Dispersion
103
Flow Cell Path Length
103
Peak Width (Response Time)
105
Sample and Reference Wavelength and Bandwidth
107
Slit Width
110
Optimizing Spectral Acquisition (DAD Only)
112
Margin for Negative Absorbance
112
Optimizing Selectivity
113
Quantifying Coeluting Peaks by Peak Suppression
113
Ratio Qualifiers for Selective Detection of Compound Classes
115
6 Troubleshooting and Diagnostics
117
Overview of the Module's Indicators and Test Functions
118
Status Indicators
119
Power Supply Indicator
119
Module Status Indicator
120
User Interfaces
121
Agilent Lab Advisor Software
122
7 Error Information
123
What Are Error Messages
125
General Error Messages
126
Timeout
126
Shutdown
127
Remote Timeout
127
Lost CAN Partner
128
Leak Sensor Short
128
Leak Sensor Open
129
Compensation Sensor Open
129
Compensation Sensor Short
130
Fan Failed
130
Leak
131
Additional Information
132
Open Cover
133
Cover Violation
133
Detector Error Messages
134
Visible Lamp Current
134
Visible Lamp Voltage
134
Diode Current Leakage
135
UV Lamp Current
135
UV Lamp Voltage
136
UV Ignition Failed
136
UV Heater Current
137
Calibration Values Invalid
137
Holmium Oxide Test Failed
138
Illegal Temperature Value from Sensor on Main Board
138
Illegal Temperature Value from Sensor at Air Inlet
139
Wavelength Recalibration Lost
139
Heater at Fan Assembly Failed
140
Heater Power at Limit
140
DSP Not Running
141
No Run Data Available in Device
141
Instrument Logbook
142
8 Test Functions
143
Self-Test
144
Filter Test
145
Test Evaluation
147
Intensity Test
148
Test Evaluation
148
Holmium Oxide Test
151
Test Evaluation
151
ASTM Drift and Noise Test
154
Test Evaluation
154
Cell Test
156
Test Evaluation
156
Using the Built-In Test Chromatogram
158
Procedure Using the Agilent Lab Advisor
158
Wavelength Verification and Calibration
160
9 Maintenance
163
Introduction to Maintenance
164
Cautions and Warnings
165
Overview of Maintenance
167
Cleaning the Module
168
Exchanging a Lamp
169
Exchanging a Flow Cell
172
Maintenance of Standard, Semi-Micro or Micro Flow Cell
176
Maintenance of High Pressure Flow Cell
180
Replacing Capillaries on a Standard Flow Cell
182
Replacing Capillaries on a Semi-Micro and Micro Flow Cell
188
Nano Flow Cell - Replacing or Cleaning
192
Cleaning or Exchanging the Holmium Oxide Filter
197
Correcting Leaks
200
Replacing Leak Handling System Parts
201
Replacing the Compactflash Card (G1315C/G1365C Only)
202
Replacing the Module's Firmware
203
10 Parts for Maintenance
205
Overview of Maintenance Parts
206
Standard Flow Cell
208
Standard Flow Cell Bio-Inert
210
Semi-Micro Flow Cell Parts
212
Micro Flow Cell
214
Prep Flow Cell - SST
216
Prep Flow Cell - Quartz
218
Nano Flow Cells
220
High Pressure Flow Cell
224
Accessory Kits
226
11 Identifying Cables
229
Cable Overview
230
Analog Cables
232
Remote Cables
234
BCD Cables
237
CAN/LAN Cables
239
Agilent 1200 Module to PC
240
12 Hardware Information
241
Firmware Description
242
Electrical Connections
245
Serial Number Information (ALL)
246
Rear View of the Module
246
Interfaces
247
Interfaces Overview
250
Setting the 8-Bit Configuration Switch
254
Special Settings
256
Instrument Layout
258
Early Maintenance Feedback (EMF)
259
13 LAN Configuration
261
What You Have to Do First
262
TCP/IP Parameter Configuration
263
Configuration Switch
264
Initialization Mode Selection
265
Dynamic Host Configuration Protocol (DHCP)
269
General Information (DHCP)
269
Setup (DHCP)
270
Link Configuration Selection
272
Automatic Configuration with Bootp
273
About Agilent Bootp Service
273
How Bootp Service Works
274
Situation: Cannot Establish LAN Communication
274
Installation of Bootp Service
275
Two Methods to Determine the MAC Address
277
Assigning IP Addresses Using the Agilent Bootp Service
278
Changing the IP Address of an Instrument Using the Agilent Bootp Service
281
Storing the Settings Permanently with Bootp
283
Manual Configuration
284
With Telnet
285
With the Instant Pilot (G4208A)
289
14 Appendix Safety Information
292
The Waste Electrical and Electronic Equipment (WEEE) Directive (2002/96/EC)
295
Radio Interference
296
Sound Emission
297
UV-Radiation
298
Solvent Information
299
Declaration of Conformity for HOX2 Filter
301
Installation of Stainless Steel Cladded PEEK Capillaries
302
First Step: Finger-Tight Fitting
303
Second Step: Installation to Connector
303
Removing Capillaries
307
Agilent Technologies on Internet
308
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