Summary of Contents for nanalysis NMReady 60e
- Page 1 NMReady™ 60e Quick Start Guide Nanalysis Corporation 1 of 17 Copyright 2016 ▪ Nanalysis Corporation...
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Page 2: What's In This Guide
• Operating recommendations • Network requirements • Powering up the instrument • Site adjustments • Solvent reference tubes and solvent management • Broken tube removal • Shipping the instrument • The Sample Warmer 2 of 17 Copyright 2014 ▪ Nanalysis Corporation... - Page 3 • Remove foam inserts and accessories from the plastic case first • Have 1 strong person lift the instrument out of the case, placing very carefully on chosen bench • Do not slide instrument along bench surface 3 of 17 Copyright 2014 ▪ Nanalysis Corporation...
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Page 4: Parts Checklist
For removing broken NMR tubes Sample warmer and power cord For keeping samples and solvent references at the ideal temperature. Performance can be degraded if un-heated samples and/or references are used in the spectrometer. 4 of 17 Copyright 2014 ▪ Nanalysis Corporation... -
Page 5: Site Requirements
• Should not be within 2.5 meters of electric motors or large masses of moving metal. • If situated on a desk or bench it should not be over the drawer stack, as moving steel will affect magnetic gradients. 5 of 17 Copyright 2014 ▪ Nanalysis Corporation... -
Page 6: Operating Recommendations
– Suggested times for using Standby Shimming are: overnight, over weekends, during holidays and through work periods when the NMReady will not be required for an extended period of time. For example, turn on standby shimming when leaving for the day. 6 of 17 Copyright 2014 ▪ Nanalysis Corporation... -
Page 7: Network Requirements
LAN and/or Internet connection. • Internet-based features include: – sharing the instrument’s screen with a customer service agent for troubleshooting or training – proactive performance monitoring with Nanalysis customer service • LAN-based features include: – uploading spectra to a shared folder –... - Page 8 4. It is a good idea to turn on for turning on the sample warmer the touch (see last pages panel display at the same time of this document) as the NMReady 8 of 17 Copyright 2014 ▪ Nanalysis Corporation...
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Page 9: Installation Wizard
• Please follow the instructions as the wizard steps through the install procedure • A typical install will take 3-5 hours • When the install is complete the main screen will be displayed 9 of 17 Copyright 2014 ▪ Nanalysis Corporation... -
Page 10: Main Screen
Main Screen • “Go” will be greyed-out until a solvent is selected 10 of 17 Copyright 2014 ▪ Nanalysis Corporation... - Page 11 – To a new room or building, perform a Site Installation ( press Setup button and go to Service > Scripts • When powering off/on the instrument – Wait for all automated tests to complete 11 of 17 Copyright 2014 ▪ Nanalysis Corporation...
- Page 12 The references are used to shim the instrument to a specific solvent. Supported Solvents Blue O, d-Chloroform, d2-dichloromethane d6-benzene, d6-dimethylsulfoxide, DMSO, d8-toluene, d8-tetrahydrofuran Yellow Pink d4-acetic acid, d6-acetone, d3-acetonitrile, d4-methanol, d-trifluoroacetic acid 12 of 17 Copyright 2014 ▪ Nanalysis Corporation...
- Page 13 Solvent Management To add or remove solvents from the instrument's solvent list go to ‘Setup’… ‘System’… ‘Solvents’ 13 of 17 Copyright 2014 ▪ Nanalysis Corporation...
- Page 14 (e.g. Isopropyl alcohol). Wait for the solvent to dry before plugging the power cord in. Never place the spectrometer completely upside down 14 of 17 Copyright 2014 ▪ Nanalysis Corporation...
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Page 15: Shipping The Instrument
Secure with screws, not nails. • Ship the crate as fragile and “dangerous goods” (DG) – Product is not dangerous but the DG designation will ensure better treatment in terms of temperature stability and shock/vibration 15 of 17 Copyright 2014 ▪ Nanalysis Corporation... - Page 16 • Any sample you are testing should also be placed in the warmer at least 5 minutes before usage • Performance can be degraded if un-heated samples and/or references are used. 16 of 17 Copyright 2014 ▪ Nanalysis Corporation...
- Page 17 For transfer of log files NMRServer™ Further information for your IT Dept - The Mac ID of the instrument is available from your sales rep - The instrument obtains its IP address using DHCP 17 of 17 Copyright 2014 ▪ Nanalysis Corporation...
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