A&D MF-50 Instruction Manual
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A&D MF-50 Instruction Manual

A&D MF-50 Instruction Manual

A&d moisture analyzer instruction manual ms-70 mx-50 mf-50 ml-50
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Summary of Contents for A&D MF-50

  • Page 1 ふ MS-70 MX-50 MF-50 ML-50 1WMPD4000477F...
  • Page 2 This manual and Marks All safety messages are identified by the following, “WARNING” or “CAUTION”, of ANSI Z535.4 (American National Standard Institute: Product Safety Signs and Labels). The meanings are as follows: WARNING CAUTION This is a hazard alert mark. This mark is the IEC417 mark for "Caution.

  • Page 3: Table Of Contents

    7.1.4. Drying Program (Heating Pattern and Drying Temperature)... 28 7.1.5. Measurement Unit ... 29 7.2. Procedures to Store a Measurement Program ...30 7.2.1. Standard Drying ... 30 7.2.2. Ramp Drying ... 33 7.2.3. Step Drying ... 37 MS-70 / MX-50 / MF-50 / ML-50...
  • Page 4 14.2. Replacement of the Halogen Lamp ...64 14.3. Factory Settings...65 14.3.1. Operation ... 65 14.4. Troubleshooting...66 14.5. Error Message ...67 Specifications... 68 15.1. Dimensions ...69 15.2. Accessories and Peripheral Equipment...70 Index ... 71 MS-70 / MX-50 / MF-50 / ML-50...

  • Page 5: Safety And Compliance

    Avoid leaving the analyzer in direct sunlight, as that could cause discoloration of the case or a malfunction. MS-70 / MX-50 / MF-50 / ML-50 mark, because they may get very hot and...
  • Page 6 This device features radio interference suppression and safety regulation in compliance with the following Council Directives Council directive 89/336/EEC Council directive 73/23/EEC EN61326 Emission and Immunity. EN61326 EMC directive EN61010-1 Low voltage directive MS-70 / MX-50 / MF-50 / ML-50...
  • Page 7 MS-70 / MX-50 / MF-50 / ML-50...

  • Page 8: Precautions

    Install the analyzer where it not affected by heaters or air conditioners. Ensure a stable power source. Keep the analyzer away from equipment that generates magnetic fields. Discharge static electricity. The Rated Voltage of Halogen Lamp AC 120 V AC 240 V MS-70 / MX-50 / MF-50 / ML-50...

  • Page 9: During Use

    During and after measurement, parts of the analyzer become very hot. Do not put flammable matter near the analyzer. Do not put any thing on the heater cover. MS-70 / MX-50 / MF-50 / ML-50 Pan support Pan handle Breeze break ring...

  • Page 10: After Use And Maintaining The Analyzer

    Do not use organic solvents to clean the analyzer. Do not disassemble or remodel the analyzer. key is always effective. If there is an error or danger, STOP Screw Glass housing Screw Glass-housing Halogen lamp MS-70 / MX-50 / MF-50 / ML-50...

  • Page 11: Outline And Features

    The software, " WinCT", a standard accessory for the MF-50, is communication software for transmitting data to a computer using Microsoft Windows. MS-70 / MX-50 / MF-50 / ML-50 drying temperature and accuracy.
  • Page 12 The analyzer can calibrate the weighing sensor (Use special mass.) and drying temperature (Use temperature calibrator for MS-70 and MX-50 except MF-50 and ML-50). The analyzer can output the data required at GLP, GMP and ISO at the end of the calibration.

  • Page 13: Packing List And Names Of Each Part

    Fuse, T6.3A 250V Caution Please confirm that the analyzer is correct for your local voltage, receptacle type and the power cord. MS-70 / MX-50 / MF-50 / ML-50 Grips of heater cover Grip of pan handle Power supply voltage label...

  • Page 14: Accessory List

    Display cover Power cord RS-232C serial interface cable Test sample Sodium tartrate dihydrate, 30g Glass fiber sheets Disposable aluminum foil pan Spoon Tweezers Spare fuse, T100mA 250V Spare fuse, T6.3A 250V MF-50 ML-50 WinCT MS-70 / MX-50 / MF-50 / ML-50...

  • Page 15: Display And Keys

    D/W/D Heating pattern #1 Standard drying Ramp drying Step drying Quick drying MS-70 / MX-50 / MF-50 / ML-50 State and Meaning At gram display Preset time is displayed at timer mode At measurement Analysis time At gram display Set temperature of sample pan...
  • Page 16 Sample needs at least 0.1 g or more to start measurement. Stop current measurement Sets the display to zero in the unit of gram. Cancel key. Gram display Target quantity Target quantity Preset termination value of analyzing mode Preset time MS-70 / MX-50 / MF-50 / ML-50...

  • Page 17: Preparations

    Caution For the disposable aluminum foil pan, place it on the sample pan. MS-70 / MX-50 / MF-50 / ML-50 The Rated Voltage of the Halogen Lamp AC 120 V AC 240 V...

  • Page 18: Setting The Clock And Calendar

    Cl adj Cl adj To time 02. 0 4. 1 5 Date adjustment 02. 0 4. 1 5 12:34:56 Time adjustment 12:34:56 MS-70 / MX-50 / MF-50 / ML-50 0. 0 00 0. 0 00...

  • Page 19: Proper Operation For Precision Measurement

    Check the activation of the halogen lamp with the operation indicator. Example: If low heating temperature is set, the brightness of halogen lamp becomes dark. MS-70 / MX-50 / MF-50 / ML-50 2 g at least key to display the zero value before...

  • Page 20: The Glass Fiber Sheets

    This accessory (AX-MX-32-1) is a package of 100 glass fiber sheets. This accessory is inclued in the packing for MS-70, MX-50 and MF-50. Purchase this accessory by your order for ML-50. Use the glass fiber sheet (AX-MX32-1) for high surface tension liquid sample.

  • Page 21: Measurement Procedure

    Measurement unit... Moisture content is based Minimum scale value of % display... 0.01 % Minimum scale value of gram display... 0.001 g Data memory function ... Not used MS-70 / MX-50 / MF-50 / ML-50 Minimum scale 0.001 % 0.01 %/min 0.01 %...
  • Page 22 ↑ key to select ACCURACY. key to select the drying RESET RESET Standard mode ACCURACY Standard drying ML-50 does not display Temperature key. MS-70 / MX-50 / MF-50 / ML-50 Preparation Close...
  • Page 23 If changing the condition, proceed to step 2. The sample pans can be washed and reused. There is the Reference card on the bottom of the analyzer. MS-70 / MX-50 / MF-50 / ML-50 Range of proper sample Sample needs more than 0.1 g.

  • Page 24: Quick Mode Operation

    0.05 %/min 0.10 %/min 0.20 %/min 0.20 %/min 0.50 %/min 0.10 %/min 0.20 %/min 0.20 %/min 0.50 %/min 0.20 %/min 0.50 %/min 0.50 %/min 1.00 %/min ↔ Quick measurement , Automatic selection) MOIST D/W/D MS-70 / MX-50 / MF-50 / ML-50...
  • Page 25 10. When displaying a stable value, Press the Avoid mechanical vibration, breeze and environmental noise during measurement. If it deviates from zero display, press the MS-70 / MX-50 / MF-50 / ML-50 key to display an analysis key to select ↓...
  • Page 26 Range of proper sample Sample needs more than 0.1 g. Significant sample is indicated segment. key is pressed, ENTER START key while SELECT No good Drying temperature Drying rate Analysis time Result Remove sample MS-70 / MX-50 / MF-50 / ML-50 Good Close...

  • Page 27: Program Number

    2. Press the key to select a program number ↓ ↑ 3. Press the ENTER MS-70 / MX-50 / MF-50 / ML-50 20 sets PROG 1 to 20 10 sets PROG 1 to 10 05 sets PROG 1 to 5 key in gram display.

  • Page 28: Measurement Programs

    Standard drying Ramp drying Step drying Quick drying Standard drying Ramp drying Step drying key. Max. Drying Program Drying Temperature MX-50 ML-50 MS-70 MF-50 ML-50 Standard drying 30°C 50°C 200°C 200°C Standard drying MS-70 / MX-50 / MF-50 / ML-50...

  • Page 29: Accuracy Of The Standard Mode And Quick Mode

    Sample quantity Quick Mode Model MS-70 MX-50 Preset Termination value MF-50 ML-50 Sample quantity MS-70 / MX-50 / MF-50 / ML-50 Minimum scale 0.001 % 0.01 %/min 0.01 % 0.02 %/min 0.1 % 0.10 %/min 0.01 % 0.02 %/min 0.1 % 0.10 %/min...

  • Page 30: Analyzing Mode Of The Automatic Mode

    Temperature2 Temperature2 Temperature1 Time1 Stage 1 Stage 2 Range MF-50 Available Available range (Factory setting) (Factory setting) Unavailable item Quick Mode Time Temperature Time1 Time2 Stage 2 200°C 3 min. Temperature MS-70 / MX-50 / MF-50 / ML-50 ML-50 range...

  • Page 31: Measurement Unit

    Drying Temperature at the Sample Pan Drying temperature range for MS-70... 30°C to 200°C, 1°C interval. Drying temperature range for MX-50, MF-50 and ML-50 ... 50°C to 200°C, 1°C interval. When a measurement is started and one hour passes, the maximum temperature is automatically regulated to 160°C for safety.

  • Page 32: Procedures To Store A Measurement Program

    ↓ key to use the number. and returns to the Drying temperature Time Timer Mode % MOIST /W/D PROG 1 0. 0 00 Program number PROG " 2 PROG 2 0. 0 00 MS-70 / MX-50 / MF-50 / ML-50...
  • Page 33 ) with the ↓ Set the Minimum Scale Value of the % Display 12. Select % display with the Select 0.01 [%] with the MS-70 / MX-50 / MF-50 / ML-50 key to select a symbol, it will key. ↓ ↑...
  • Page 34 SELECT key. ↓ ↑ key. RESET Minimum scale value of gram " 0 . " 0 " 0 " 1 display 0. 0 00 Gram display of weighing mode MS-70 / MX-50 / MF-50 / ML-50...

  • Page 35: Ramp Drying

    If the data memory function is active, the data memory number (MEM) is displayed in place of the program number (PROG). MS-70 / MX-50 / MF-50 / ML-50 (ML-50 can not select ramp drying) Final drying temperature Heating pattern...Ramp drying ( Final drying temperature...160°C...
  • Page 36 Standard mode Manual mode Measurement unit Minimum scale value of % display Minimum scale value of gram display MS-70 / MX-50 / MF-50 / ML-50 Standard mode 0. 0 00 0. 0 00 0. 0 00 Automatic mode " 0 ." 0 " 5 %/min "...
  • Page 37 Caution If the data memory function is active, the data memory number (MEM) is displayed in place of the program number (PROG). MS-70 / MX-50 / MF-50 / ML-50 key to store the new parameters of key. RESET Final drying temperature Drying time Heating pattern...Ramp drying (...
  • Page 38 " 0 . " 0 " 0 " 1 display 160°C 0. 0 00 10.0 min Gram display of weighing mode MS-70 / MX-50 / MF-50 / ML-50 " M " O " I " S " T " % " / " W...

  • Page 39: Step Drying

    Caution If the data memory function is active, the data memory number (MEM) is displayed in place of the program number (PROG). MS-70 / MX-50 / MF-50 / ML-50 (ML-50 can not select step drying) Drying temperature 2 Time Stage 2 Heating pattern...Step drying (...
  • Page 40 " 5 ." 0 min Drying temperature 2 " 1 " 6 " 0 °C Preset termination value Standard mode Manual mode Measurement unit MS-70 / MX-50 / MF-50 / ML-50 Standard mode Automatic mode " 0 ." 0 " 5 %/min "...
  • Page 41 Measurement unit ...Moisture content Minimum scale value during measurement ..0.01 % Minimum scale value of the gram display...0.001 g Sample quantity...Approximately 5 g Data memory function ...Not used MS-70 / MX-50 / MF-50 / ML-50 key. SELECT key. ↓ ↑...
  • Page 42 " 5 ." 0 min Drying Temperature 2 key. " 1 " 6 " 0 °C Time 2 " 1 " 0 ." 0 min MS-70 / MX-50 / MF-50 / ML-50 0. 0 00 0. 0 00 0. 0 00...
  • Page 43 Pressing the key, the weighing mode is automatically displayed. When PROG 6 is recalled, the settings can be used. To cancel the new parameters and return to the weighing mode, press the MS-70 / MX-50 / MF-50 / ML-50 key. SELECT key. ↑...

  • Page 44: Check Function

    CH pa55 CH no error 0 Ht err 0. 0 00 Press and hold Do not put sample Preparation Checking CH ..Good result CH pa55 0. 0 00 Weighing mode MS-70 / MX-50 / MF-50 / ML-50...

  • Page 45: Test Sample (Sodium Tartrate Dihydrate)

    The test sample can not be used repeatedly. Dispose of it as flammable matter. In case of MS-70 MX-50 and MF-50, test sample is included in these packing list. In case of ML-50, purchase the test sample of accessory.

  • Page 46: Connecting To A Printer

    Analyzer settings pU5e info Connect to RS-232C interface of the analyzer. AD-8121B Dip switch settings MODE 3 Dump printing MODE 1 MODE 2 Interval printing MODE 3 Dump printing Accessory cable of AD-8121B MS-70 / MX-50 / MF-50 / ML-50...

  • Page 47: Print Samples

    -ü-ü-ü-ü-ü-ü-ü- ü SIGNATURE -ü-ü-ü-ü-ü-ü-ü- ü ID number can be changed. Refer to "12.1. Identification Number (ID No.)" MS-70 / MX-50 / MF-50 / ML-50 Description When pressing the ENTER Data is outputted after measurement automatically. Result is outputted only. Approx. two seconds interval in each line.

  • Page 48: Example To Print Selected Items

    "signature space". key, the result is outputted. ENTER 0. 0 00 Press and hold li5t Print 0. 0 00 0. 0 00 Press and hold Print 0. 0 00 MS-70 / MX-50 / MF-50 / ML-50 li5t li5t...
  • Page 49 TIMEüüüü13:24:57 REMARKS ü-ü-ü-ü-ü-ü-ü-ü- SIGNATURE ü-ü-ü-ü-ü-ü-ü-ü- ID number can be changed. Refer to "12.1. Identification Number (ID No.)" ＊1: MS-70 / MX-50 / MF-50 / ML-50 Factory Product Serial number ID number. ＊1 PROG No. Analysis mode. Refer to 9.1.3 Drying program. Refer to 9.1.3...

  • Page 50: Explanation For Print Item

    Analyzing mode to finish measurement Timer mode Analysis time Manual mode Standard drying Drying temperature Ramp drying Final drying temperature Step drying Drying temperature of stage 1 Drying temperature of stage 2 Quick drying Drying temperature MS-70 / MX-50 / MF-50 / ML-50...
  • Page 51 TIMEüüüü13:24:57 "Remarks Space" For instance: This space can use for a comment about samples. REMARKS ü-ü-ü-ü-ü-ü-ü-ü- "Signature Space" SIGNATURE ü-ü-ü-ü-ü-ü-ü-ü- MS-70 / MX-50 / MF-50 / ML-50 A Part of Print UNITüüüüMOIST/üW UNITüüüüMOIST/üD UNITüüüRATIOüD/W UNITüüüRATIOüW/D UNITüüüüüüüüüüüg D: Dried sample mass...

  • Page 52: Ms-70 / Mx-50 / Mf-50 / Ml

    The MS-70 and MX-50 have the following standard accessory cable for RS-232C. If it is necessary to connect a cable to the MF-50 and ML-50, purchase the cable of accessory AX-MX-40. If purchasing the RS-232C cable on the market, check the interface connections and type.

  • Page 53: Rs-232C Serial Interface

    2: Signal names of the analyzer side are the same as the DTE side with TXD and RXD reversed. 3: RTS and CTS control are not used. CTS output is HI always. MS-70 / MX-50 / MF-50 / ML-50 EIA RS-232C Asynchronous, bi-directional, half duplex...

  • Page 54: Output Format

    Negative Overload Format (Too light weighing, Header Polarity Overload Moisture Content (during weighing or after weighing) In case of the MS-70 Header Moisture content In case of the MX-50 or MF-50 Header Moisture content In case of the ML-50 Header Moisture content Unit Terminator Terminator...

  • Page 55: Command

    The format consists of nineteen characters except the terminator. In case of the MS-70 Header Moisture content 160°C at sample pan In case of the MX-50 or MF-50 Header Moisture content 160°C at sample pan In case of the ML-50 Header Moisture content 160°C at sample pan...

  • Page 56: Data Memory Function

    MF-50 ML-50 50 data 30 data data 1 data 0 is displayed. Press and hold Cl adj data Store result data " 1 MS-70 / MX-50 / MF-50 / ML-50 0. 0 00 0. 0 00...

  • Page 57: Output All Data At One Time

    ↓ ↑ 5. Press the ENTER 6. When deleting is finished, MS-70 / MX-50 / MF-50 / ML-50 key to display ENTER key to display out " n " o out " g " o key to output the data in order.

  • Page 58: Calibration

    J K L M N O P Q key to enter the function SELECT is displayed. key to display key. key to return to the weighing mode. Space -(hyphen) 0. 0 00 Press and Cl adj lab-123 0. 0 00 MS-70 / MX-50 / MF-50 / ML-50...

  • Page 59: Calibration Of The Weighting Sensor

    If the report for GLP, GMP and ISO is to be output (Refer to page 61), The output condition for the report is selected in the function table. MS-70 / MX-50 / MF-50 / ML-50 key to display PROGRAM key to display...
  • Page 60 Calibration report is printed at "Calibration of the Weighting Sensor" and "Calibration of Drying info 2 Temperature". Dump print (Received data is printed as it is) Manufacture Model Serial number ID number Date Time Calibration type Calibration mass Signature MS-70 / MX-50 / MF-50 / ML-50...

  • Page 61: Calibration Of Drying Temperature (For Ms-70 And Mx-50)

    " 1 " 0 " 0 °C thermometer value using the 97°C) 9. Press the ENTER to start the 160°C measurement. MS-70 / MX-50 / MF-50 / ML-50 PROGRAM key to display t-Cal key. key to start the 100°C blinking value key.
  • Page 62 100°C target value 160°C target value Signature Buzzer 160℃ " 1 " 6 " 0 ℃ 160℃ " 1 " 6 " 2 ℃ 0. 0 00 0. 0 00 measurement value measurement value MS-70 / MX-50 / MF-50 / ML-50...

  • Page 63: Function Table

    4: Refer to "9.1.2. Example To Print Selected Items". 5: Calibration report is outputted in "Calibration of the Weighting Sensor" and "Calibration of Drying Temperature". MS-70 / MX-50 / MF-50 / ML-50 Param- eter Set date and time for the built-in clock.

  • Page 64: Operation

    " 0 ○ Last parameter New parameter ○ prt " 1 data 0. 0 00 0. 0 00 Cl adj Last parameter dp 0 ○ New parameter dp 1 0. , 0 00 MS-70 / MX-50 / MF-50 / ML-50...

  • Page 65: Maintenance

    Do not touch the temperature sensor that is at the side of halogen lamp. If the surface is touched, it may be the cause of a drying temperature error. MS-70 / MX-50 / MF-50 / ML-50 Halogen lamp Metal reflector...

  • Page 66: Replacement Of The Halogen Lamp

    Do not pinch the wire between the glass housing and lid. Accessory number the Halogen Lamp AX-MX-34-120V AC 120 V AX-MX-34-240V AC 240 V There is downward projection. Screw Heater Unit Halogen lamp Hook Connector Wire Read rated voltage. Glass-housing MS-70 / MX-50 / MF-50 / ML-50 Screw Holder Hook...

  • Page 67: Factory Settings

    RESET 6. Press the ENTER is displayed. 7. Press the RESET MS-70 / MX-50 / MF-50 / ML-50 key to enter the function SELECT key to display key to enter the item. Clr " g " o key with Clr "...

  • Page 68: Troubleshooting

    Halogen Lamp AC 120 V AC 240 V Power supply voltage label Fuse, T100mA 250V Fuse, T6.3A 250V MS-70 / MX-50 / MF-50 / ML-50 Maximum height of mass is 26 mm. Halogen lamp Read rated voltage Accessory number...

  • Page 69: Error Message

    15 seconds, the weighing mode is automatically displayed. Full Memory The number of results stored in memory has reached the upper limit. Clear the data to store the new results. Refer to "11. Data Memory Function". MS-70 / MX-50 / MF-50 / ML-50...

  • Page 70: Specifications

    0.2 % 0.5 % 0.002 g 0.005 g 0.05%, 0.1%, 0.1 %, 0.002g 0.002g Standard drying Standard drying Standard drying Standard drying 10 sets 50 results 30 results φ85 mm MS-70 / MX-50 / MF-50 / ML-50 ML-50 5 sets...

  • Page 71: Dimensions

    3: Please confirm that this analyzer is correct for your local voltage and receptacle type and the power cord. 4: Application software for Windows. 15.1. Dimensions MS-70 / MX-50 / MF-50 / ML-50 MS-70 MX-50 AC100V to 120V 3A or AC200V to 240V 1.5A, 50Hz or 60Hz, Approximately 400W 215(W) x 320(D) x 173(H)mm, 8.46(W) x 12.60(D) x 6.81(H)in.

  • Page 72: Accessories And Peripheral Equipment

    Statistical function, interval printing, chart printing, 5x7 dot, height 2.5mm/01.in., 16 characters/line AC adapter or alkaline batteries Order number AX-MX-30 AX-MX-31 AX-MX-32-1 AX-MX-32-2 AX-MX-33 AX-MX-34-120V AX-MX-34-240V AX-MX-35 AX-MX-36 AX-MX-37 AX-MX-38 AX-MX-39 AX-MX-40 AX-MX-41 AX-MX-42 AX-MX-43 MS-70 / MX-50 / MF-50 / ML-50...

  • Page 73: Index

    Cl adj -----------------------------------------61 Cl err -----------------------------------------67 Clo5e --------------------------------------42, 67 Clock ---------------------------------------16, 61 Clr -----------------------------------------55, 61 Clr go -----------------------------------------65 MS-70 / MX-50 / MF-50 / ML-50 Comma----------------------------------------- 61 Command ------------------------------------- 53 Continuous measurement ------------------ 17 CR----------------------------------------------- 52 CTS --------------------------------------------- 51 data --------------------------------------- 54, 61...
  • Page 74 U-a ----------------------------------------- 14, 26 U-m ----------------------------------------- 14, 26 Unit----------------------------------------- 29, 52 U-t ----------------------------------------- 14, 26 Weighing sensor------------------------ 56, 57 Wet sample mass --------------------------- 29 WinCT ---------------------------------------9, 50 WinCT-Moisture --------------------------9, 50 ymd ---------------------------------------------- 16 Zero display----------------------------------- 14 MS-70 / MX-50 / MF-50 / ML-50...

This manual is also suitable for:

Ml-50Ms-70Mx-50

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