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Table of Contents
Related Manuals for SPECTRO XEP05
Summary of Contents for SPECTRO XEP05
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Page 3: Table Of Contents
Switching off the instrument ....................31 Standby mode ........................32 Measuring procedure ......................33 5.6.1 Preparing the measuring procedure ..............33 How to measure different samples ..............34 SPECTRO XEPOS — 19.01.2017 — 3... - Page 4 6.11 Troubleshooting ........................ 51 Spare parts and consumables ................55 De-commissioning .................... 55 Manufacturer address ..................55 EC Declaration of Conformity ................56 — 4 SPECTRO XEPOS — 19.01.2017...
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Page 5: Description Of Instrument
After the measurement is complete, the results of a sample relating to an unknown composition are displayed on the screen. The sample material may be solid, liquid or in powder form, see Chapter "How to measure different samples". SPECTRO XEPOS — 19.01.2017 — 5... -
Page 6: Overview
Depending on the application / requirement, the following expansions are available: Sample spinner Helium flushing Vacuum pump Active pile-up suppression Dust protection shutter / beam stabilization vacuum shutter — 6 SPECTRO XEPOS — 19.01.2017... -
Page 7: Instrument (Front)
Fig. 1: Front view Component Sample chamber lid Ventilation slots with filter mat Beam stop display Open/closed (Open = red/closed = green) X-ray display On/Off (On = orange/Off = off), see also Chapter 5.1.2. SPECTRO XEPOS — 19.01.2017 — 7... -
Page 8: Opening And Closing The Sample Chamber Lid
When pressing slightly against the handle, the sample chamber lid can be pushed back and locked into place. In order to open the cover, slightly press against the handle and pull on the sample chamber lid. — 8 SPECTRO XEPOS — 19.01.2017... -
Page 9: Instrument (Back)
Power In (max. 1200 W) LAN cable included in delivery) Helium supply line connection Key-operated switch On/Off Vacuum hose connection Note Set up the instrument to ensure the power isolators (switches and power cable) can be easily reached. SPECTRO XEPOS — 19.01.2017 — 9... -
Page 10: Sample Chamber
Description of instrument 1.3.4 Sample chamber Fig. 4 Component Sample tray locking device Sample tray (different models available) Analysis position (position of the sample during the measurement) Tray handle Tray screw — 10 SPECTRO XEPOS — 19.01.2017... -
Page 11: Sample Chamber - Additional Components
12 sample positions for Ø 40 mm samples with an adapter for Ø 32 mm samples 25 sample positions for Ø 20 mm samples 8 sample positions for rotating samples for Ø 40 mm samples or 6 sample positions for rotating Ø 52 mm samples SPECTRO XEPOS — 19.01.2017 — 11... -
Page 12: Safety
Caution! Ionizing radiation! Notice! Warns of activities or conditions that may adversely affect the safety or function of the instrument. Note Displays information that is important for the correct and safe use of the instrument — 12 SPECTRO XEPOS — 19.01.2017... -
Page 13: User Information
Intended use The spectrometer must only be used to analyse liquid substances or powdery materials inside special containers (e.g., cuvette, sample cup). Solid samples, e.g., metal parts, may be analyzed outside of these containers. SPECTRO XEPOS — 19.01.2017 — 13... -
Page 14: Prohibited Operating Conditions
This ensures that no broken beryllium window pieces can leave the spectrometer. Switch off the spectrometer and inform the service department of SPECTRO. The detector and the spectrometer can no longer be used. Caution! Risk of crushing injuries! When closing the sample chamber lid, there is an inherent risk of crushing injuries. - Page 15 (see also chapter 5.3.4). Three days before the deadline, a first reminder appears in the status display of the software. SPECTRO XEPOS — 19.01.2017 — 15...
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Page 16: Radiation Protection Advice
The operation of the instrument may require official approval in other countries. Compliance with the national safety and approval regulations in force in your country and/or state is mandatory! Please contact the responsible local approval authority. — 16 SPECTRO XEPOS — 19.01.2017... -
Page 17: Technical Data
1.0 – 3.0 bar; (15 – 44 psi) ≥ 99.996% (4.6) Quality Consumption typically 4.5 L per analysis Vacuum (option) End pressure/operating pressure < 5 mbar (0.07 psi) Voltage supply 110 V/230 V (instrument-controlled) SPECTRO XEPOS — 19.01.2017 — 17... -
Page 18: Transportation/Setting-Up
All necessary cables and hoses are included in the delivery. If the instrument is to be moved to another place of installation after set-up, there is a risk of damaging the instrument. Contact the SPECTRO Service Department in this matter. — 18 SPECTRO XEPOS — 19.01.2017... -
Page 19: Storage
Input pressure 1.0 to 3.0 bar; (15 to 44 psi) Gas is supplied through a PTFE hose included in SPECTRO's scope of supply: Dimensions OD/ID = 6/4 mm, length 3 m (~ 10 ft) This hose is inserted into the rear panel of the spectrometer, see page 9. -
Page 20: Vacuum (Option)
To do this, fasten the vacuum hose with the clamps at both connecting points. Fig. 8 Use the power cable to connect the vacuum pump and the instrument. The vacuum pump is now connected. Fig. 9 — 20 SPECTRO XEPOS — 19.01.2017... -
Page 21: Uninterruptible Power Supply - Ups (Option)
Fig. 10 Component Component UPS "ON/OFF" switch Automatic circuit breaker 6 A "Turn off alarm signal" switch PC communication port UPS power supply connection Power connection for instruments SPECTRO XEPOS — 19.01.2017 — 21... - Page 22 Connect all components with the UPS (spectrometer, PC, monitor, etc.) Connect the UPS with the power supply. Switch on the UPS. Switch on the components (spectrometer, PC, monitor, etc.) The UPS is now installed. — 22 SPECTRO XEPOS — 19.01.2017...
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Page 23: Operation
Display for information from the program and the instrument Sample data table Input fields for sample data Sample Display of the sample position, the spectrum, and the tray/spectrum/result results of the analyses Buttons Buttons for controlling the measurements SPECTRO XEPOS — 19.01.2017 — 23... -
Page 24: Beam Stop Display On The Instrument
Beam Stop open HV generator switched off This condition may occur during the start-up test red light orange light Beam Stop open HV generator switched on Measurement mode — 24 SPECTRO XEPOS — 19.01.2017... -
Page 25: Switching On The Instrument
Turn the key-operated switch on the spectrometer (see figure, page 9, Pos. 7) into its horizontal position. Switch on the computer. The operating system is started. Click on the "XRF Analyzer Pro" button; this will start the routine dialog. A login window opens: SPECTRO XEPOS — 19.01.2017 — 25... - Page 26 (see Chapter "Initialization of the stepping motors"). The instrument is switched on. In order to ensure stable measurement conditions, it is highly recommended to wait 20 minutes before starting the measurements. — 26 SPECTRO XEPOS — 19.01.2017...
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Page 27: Proceed With The Start-Up Test
(open/closed). If the sample chamber lid is closed, you will be prompted to open it: If the sample chamber was open when the instrument was switched on, this step will be omitted and the software will skip this procedure. SPECTRO XEPOS — 19.01.2017 — 27... -
Page 28: Checking The Safety Circuit On The Filter Changer ("Beam Stop")
Beam Stop are checked autonomously by the instrument's software. During this procedure, the software displays an appropriate message: After the safety test was completed successfully, the stepping motors that are integrated into the spectrometer, are initialized. — 28 SPECTRO XEPOS — 19.01.2017... -
Page 29: Initialization Of The Stepping Motors
If there is no sample tray inside the sample chamber, click on "OK, Plate Removed". Follow the instructions on the screen. Details about the content and the progress of the initialization process can be seen on the messages. SPECTRO XEPOS — 19.01.2017 — 29... -
Page 30: Automatic Verification Of The Safety Circuits After One Month
Switch off the device at the key-operated switch and turn it on again after three seconds, not sooner. Subsequently, connect the device to the software. The automatic check of the safety circuits starts as described in the chapter 5.3.1. — 30 SPECTRO XEPOS — 19.01.2017... -
Page 31: Switching Off The Instrument
This procedure is also required if the instrument is not to be used afterwards. To switch off the instrument, proceed as follows: Open the instrument server that is installed on the computer and select "Shutdown". A security question will be asked. Confirm the question with "Yes". SPECTRO XEPOS — 19.01.2017 — 31... -
Page 32: Standby Mode
If the spectrometer was shut down for more than one month, the X-ray tube must be run under standby conditions for at least 1 hour. Start measuring only after this period. — 32 SPECTRO XEPOS — 19.01.2017... -
Page 33: Measuring Procedure
Adapter for Ø 32 samples "Liquid protect cup" Ensure that only such samples are present on the sample tray that are measured under the same conditions (air, helium, vacuum). The measurement is now prepared. SPECTRO XEPOS — 19.01.2017 — 33... -
Page 34: How To Measure Different Samples
To arrive at the correct analysis, in addition to the filling height, the weighted portion of the sample (or the density, if known) must be determined and entered into the software. — 34 SPECTRO XEPOS — 19.01.2017... -
Page 35: How To Measure Powder Pallets
Ø 32mm samples. Note Glass pallets must always be measured on their "own" tray. Prior to the measurement, all dust must be cleaned off the tray. A contaminated sample tray will falsify the analysis. SPECTRO XEPOS — 19.01.2017 — 35... -
Page 36: How To Measure Large Samples
Three single sample holders are included with each delivery. Additional holders can be ordered from our SPECTRO Shop. The part number can be found on page The installation of the sample tray and the sample tray support takes place in reverse order. -
Page 37: Proceed With The Measurement
The measurement is performed automatically. Perform further measurements if required. The measurement is complete. Note Measure a reference sample at regular intervals. This will allow you to identify changes of the measurement results in good time. SPECTRO XEPOS — 19.01.2017 — 37... -
Page 38: How To Change/Remove The Sample Tray
(2). Close the locking device of the sample tray by rotating it clockwise and simultaneously lifting the device slightly. Fig. 16 The sample tray has been changed. — 38 SPECTRO XEPOS — 19.01.2017... -
Page 39: Dust Protection Shutter / Beam Stabilization Vacuum Shutter (Option)
No load of the used crystal due to humidity. This leads to a better stability of the analyzes. When measurements are performed in air or using helium flushing, the system requires at least 60 minutes to return to the state of highest stability and precision. SPECTRO XEPOS — 19.01.2017 — 39... -
Page 40: Maintenance By The Operator
In order to ensure the availability and operational safety of the equipment, we recommend having the system checked for correct operation and performance at least once per year by specialized technicians. To find contact addresses of service organizations authorized by SPECTRO go to www.spectro.com Operator maintenance plan Caution! Ionizing radiation! An X-ray tube is inside the spectrometer. - Page 41 Replace the "liquid protect cups" protective See Chapter 6.8. film. Clean the sample rotation drive (do not Use a soft brush. lubricate!). Vacuum system maintenance (optional). Changing the vacuum oil and cleaning the oil mist filter. See Chapter 4.3. SPECTRO XEPOS — 19.01.2017 — 41...
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Page 42: Energy Channel Recalibration (Mca)
The corresponding program window is displayed. Press the "Start MCA only" button and follow the instructions. The energy-channel recalibration is performed automatically. After the measurement is completed, a result window is displayed. The spectrometer is recalibrated. — 42 SPECTRO XEPOS — 19.01.2017... -
Page 43: Standardization (Global Recalibration)
Press the "Recalibration" button. A window opens. Press the "Start Recalibration" button and follow the instructions. After the measurement is completed, a result window is displayed. The standardization (global recalibration) is completed. SPECTRO XEPOS — 19.01.2017 — 43... -
Page 44: Clean The Sample Tray
Notice! Risk of damage! Improper cleaning procedures can destroy the beryllium window of the detector. Never use a vacuum cleaner or compressed air to clean the sample chamber. — 44 SPECTRO XEPOS — 19.01.2017... -
Page 45: Replacing The Adhesive Film In The Discharge Reservoir
On the other side, there is a permanent adhesive surface (with white protection layer). The adhesive film can be ordered from the SPECTRO Shop. The part number can be found on page 55. To replace the filter mat, proceed as follows: Remove the old adhesive film (1). -
Page 46: Replacing The Tray Pads
The tray pads are included with each delivery. Additional pads can be ordered from our SPECTRO Shop. The part number can be found on page 55. To replace the tray pads, proceed as follows:... -
Page 47: Insert The Film For The "Liquid Protect" Sample Cup
Place the clamping ring on the film. Fig. 21 Push the clamping ring down until the sample cup holder and the clamping ring are on the same level. Ensure the film is not crinkled. Fig. 22 SPECTRO XEPOS — 19.01.2017 — 47... - Page 48 In order to replace the film, push the tool into the gap between the sample cup holder and the clamping ring and push off the clamping ring. The film is now inserted. Fig. 23 — 48 SPECTRO XEPOS — 19.01.2017...
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Page 49: Replacing The Filter Mat
Fig. 24 The filter mat is included with each delivery. Additional mats can be ordered from our SPECTRO Shop. The part number can be found on page 55. To replace the filter mat, proceed as follows: Loosen the cover on the magnetic locks (1) by pulling downward. -
Page 50: Dust Protection Shutter / Beam Stabilization Vacuum Shutter (Option) - Clean O-Ring
(isopropyl alcohol). Do not Fig. 26 apply grease to the O-ring. In order initialize the shutter (1), select the option "Re-Initialize Shutter" in the menu item"Shutter" in the Diagnostic Tools. The O-ring has been changed. — 50 SPECTRO XEPOS — 19.01.2017... -
Page 51: Troubleshooting
The connecting cable is Connect the cable and check the not connected or not plug for correct fit. properly connected to the computer. SPECTRO XEPOS — 19.01.2017 — 51... - Page 52 There is no proper sample Place the MCA sample onto the calibration, error at the measurement correct position of the sample messages appear. position or no sample at tray. all. Defective detection Please contact your Service system. Center. — 52 SPECTRO XEPOS — 19.01.2017...
- Page 53 Please contact your Service Center. system. Powder from a Apparent contamination. Clean the sample chamber. cuvette has leaked Clean or replace the film holder. into the spectrometer. Additional contamination Please contact your Service Center. that cannot be accessed. SPECTRO XEPOS — 19.01.2017 — 53...
- Page 54 "Shutter" and click the shutter does not close option "Re-initialize shutter". the excitation The drive mechanism of Please contact your Service Center. chamber after the shutter is defective. measurement. — 54 SPECTRO XEPOS — 19.01.2017...
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Page 55: Spare Parts And Consumables
Spare parts and consumables Spare parts and consumables You can find the spare parts and consumables for this instrument under "Support - Parts Catalogue" (Service – Parts Catalogue) on our website at www.spectro.com. Part numbers of various consumables: Article Order number... -
Page 56: Ec Declaration Of Conformity
EC Declaration of Conformity EC Declaration of Conformity — 56 SPECTRO XEPOS — 19.01.2017...
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