Monitoring system for the automatic, continuous measurement and dosing control of chlorine based on the dpd colorimetric method apha 4500 cl-g and on
en iso 7393-2 (116 pages)
AMI Phosphate-II Safety Instructions AMI Phosphate-II - Operator’s Manual This document describes the main steps for instrument setup, oper- ation and maintenance. Safety Instructions General The instructions included in this section explain the potential risks associated with instrument operation and provide important safety practices designed to minimize these risks.
AMI Phosphate-II Safety Instructions 1.1. Warning Notices The symbols used for safety-related notices have the following sig- nificance: WARNING WARNING Symbols Generally, the triangular warning symbol indicates the possibili- ty of personal injury or even loss of life if instructions are not fol- lowed,.
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AMI Phosphate-II Safety Instructions ATTENTION ATTENTION Symbols The attention symbol indicates the possibility of equipment damage, malfunctions or incorrect process results if instructions are not followed. Attention general Safety goggles Safety gloves A-96.250.641 / 290312...
AMI Phosphate-II Safety Instructions 1.2. General Safety Regulations Legal The user is responsible for proper system operation. All precautions must be followed to ensure safe operation Requirements of the instrument. Spare Parts Use only official SWAN spare parts and disposables. If other parts are used during the normal warranty period, the manufacturer’s...
If the sample contains only little disinfectant concentrations, or there is the danger of biological growth, we recommend to use the optional Cleaning module from Swan which is available as an op- tion for the AMI Phosphate-II. WARNING For safe instrument installation and operation you must read...
Application This manual describes the functions of the analyzers: AMI Phosphate-II AMI Phosphate-II B Both analyzers are complete monitoring systems for the automatic continuous measurement of ortho-Phosphate. ortho-Phosphate can be found in many applications like corrosion protection in sani- tary systems and boilers or as additive to detergents.
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Sample AMI Phosphate-II B Stream As an option an inlet for two sample streams with a sample switch- ing valve can be installed onto the panel of the AMI Phosphate-II B Cleaning AMI Phosphate-II Module As an option a cleaning module is available which can be connect- ed to the AMI Phosphate-II.
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AMI Phosphate-II Product Description On-line The sample flows through the sample inlet [K] and the filter vessel [J] into the constant head [A]. Adjust the flow regulating valve so operation that always a small part of the sample flows through the overflow tube [B] into the drain [R].
AMI Phosphate-II Product Description 2.1. Instrument Specification Power Supply Voltage: 100–240 VAC (± 10%) 50/60 Hz (± 5%) or 24 VDC, isolated, (± 15%) Power consumption: max. 20 VA Sample Flow rate: min. 10 l/h requirements Sample pressure inlet: 0.15–2 bar (2–28 PSI) Temperature: 5–50 °C (41–122 °F)
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AMI Phosphate-II Product Description Dimensions Panel PVC: 400 x 850 mm Phosphate-II Mounting hole distance: 374 x 824 mm Screws: 5 mm or 6 mm diam. Weight: 9.0 kg /19.9 lbs 400 mm / 15¾” 13 mm / ½” 374 mm / 14¾”...
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AMI Phosphate-II Product Description Dimensions Panel stainless steel: 400 x 850 mm Phosphate-II B Mounting hole distance: 374 x 824 mm Screws: 5 mm or 6 mm diam. Weight: 14.0 kg /30.85 lbs 400 mm / 15¾” 13 mm / ½”...
AMI Phosphate-II Installation Installation 3.1. Installation Check List Check Instrument’s specification must conform to your AC power ratings. Do not turn on power until instructed to do so. On site require- 100–240 VAC ( 10%), 50/60 Hz ( 5%) or 24 VDC (±15%), ments isolated power outlet with ground connection and 20 VA.
AMI Phosphate-II Installation 3.2. Mounting of Instrument Panel Mount the instrument in vertical position. For ease of operation mount it so that the display is at eye-level. For dimensions see pic- ture Dimensions Phosphate-II, S. 13 3.3. Connecting Sample and Waste...
AMI Phosphate-II Installation 3.4. Electrical Connections WARNING Always turn off AC power before manipulating electric parts. Grounding requirements: Only operate the instrument from an power outlet which has a ground connection. Make sure the power specification of the instrument corre- sponds to the power on site.
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AMI Phosphate-II Installation WARNING To prevent from electrical shock, do not connect the instrument to the power unless the ground wire (PE) is connected. Do not connect unless specifically instructed to do so. WARNING The mains of the AMI Transmitter must be secured by a main switch and appropriate fuse or circuit breaker.
AMI Phosphate-II Installation 3.5. Connection Diagram Phosphate-II WARNING Use only the terminals shown in this diagram, and only for the mentioned purpose. Use of any other terminals will cause short circuits with possible corresponding consequences to material and personnel. A-96.250.641 / 290312...
AMI Phosphate-II Installation 3.6. Connection Diagram Phosphate-II B WARNING Use only the terminals shown in this diagram, and only for the mentioned purpose. Use of any other terminals will cause short circuits with possible corresponding consequences to material and personnel.
AMI Phosphate-II Installation 3.7. Install the Cleaning Module The optional cleaning module can only be used together with the AMI Phosphate-II. For installation and commissioning of the cleaning module consult the manual of the cleaning module. A-96.250.641 / 290312...
Install 2 Sample Stream The 2 sample stream option is only available for the AMI Phosphate-II B. The following description assumes that the installation of the sample stream takes place after commissioning of the monitor. Flow cell block sample stream option...
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AMI Phosphate-II Installation Sample 1 Stop sample flow. Connection 2 Switch off the instrument. 3 Empty the flow cell. 4 Remove the sample inlet tube [E] from the flow cell block [A]. 5 Screw the 2 sample stream option (G) with the two fixing screws (I) to the panel.
Mains cable to comply with standards IEC 60227 or IEC 60245; flammable rating FV1 Mains equipped with an external switch or circuit-breaker - near the instrument, - easily accessible to the operator, - marked as interrupter for AMI Phosphate-II A-96.250.641 / 290312...
Note: Use only potential-free (dry) contacts. • Terminals 30/31 at AMI Phosphate-II transmitter • Terminals 9/10 at AMI Phosphate-II B peristaltic pump If signal output is set to hold, measurement is interrupted if input is active. For programming see menu 5.3.4, S.
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AMI Phosphate-II Installation ATTENTION Heavy inductive or directly controlled loads (solenoid valves, dosing pumps) must be switched by external power relays. In this case, use the AMI relaybox which is available as an option. Small inductive loads (max 0.1A) as for example the coil of a power relay can be switched directly.
AMI Phosphate-II Installation 3.12. Signal Outputs 3.12.1 Signal Output 1 and 2 (current outputs) Note: Max. burden 510 If signals are sent to two different receivers, use signal isolator (loop isolator). Signal output 1: Terminals 14 (+) and 13 (-)
AMI Phosphate-II Installation 3.13. Interface Interface Terminal 50, 52, 53 RS232 The AMI Interface RS232 PCB is used for Logger down load and Firmware up load. For detailed information see the corresponding manual “AMI RS232 Interface”. RS232 Interface PCB Interface...
AMI Phosphate-II Instrument Setup Instrument Setup After installation according to the checklist proceed as following: 1 Prepare reagents. See Reagents for Measuring Phosphate, S. 2 Insert suction lance/level detectors 3 Lock the occlusion frames of the peristaltic pump. The peristaltic pump is ready.
AMI Phosphate-II Instrument Setup 4.2. Fill / Flush Reagent System Fill or flush the reagent tubing: upon the initial instrument setup, after refilling the reagent containers, before a system shut-down to flush the system with demin water until no more reagent is left in the system.
AMI Phosphate-II Operation Operation 5.1. Function of the Keys Exit Enter to exit a menu or command (rejecting any changes) to move back to the previous menu level to move DOWN in a menu list and to decrease digits to move UP in a menu list and to increase digits...
AMI Phosphate-II Operation 5.2. Measured Values and Symbols on the Display Display when Operating with one Sample Stream 15:20:18 21.5 23 b/s normal operation GRAB manual grab sample HOLD input closed or cal delay: Instrument on hold (shows status of signal outputs).
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AMI Phosphate-II Operation Display when Only applicable with AMI Phosphate-II B and installed 2 sample stream option. Operating with two Sample Streams 15:20:18 21.5 PO4 1 21.5 PO4 2 23 b/s normal operation HOLD input closed or cal delay: Instrument on hold (shows status of signal outputs).
AMI Phosphate-II Operation 5.3. Software Structure Main Menu Messages Diagnostics Maintenance Operation Installation Menu 1: Messages Messages Reveals pending errors as well as an event history Pending Errors (time and state of events that have occurred at an ear- Maintenance List lier point of time) and maintenance requests.
AMI Phosphate-II Operation 5.4. Changing Parameters and Values Changing The following example shows how to change the log interval: Highlight the menu item indicating the parameters Sensors Logger 5.1.2 4.4.1 parameter you want to change. Sensor type FOME Log interval 30 min Disinf.
AMI Phosphate-II Maintenance Maintenance 6.1. Maintenance Schedule WARNING Stop operation before maintenance. Stop sample flow. Shut off power of the instrument. Daily (dirty water) Check sample supply for dirt. up to every Clean all filters and strainers, if necessary.
AMI Phosphate-II Maintenance 6.2. Stop of Operation for Maintenance Before starting any maintenance work, all pipes as well as the pho- tometer and the constant head must be rinsed with clean water to remove the reagents. To rinse the system proceed as follows: 1 Put suction lances into a bucket with clean water.
AMI Phosphate-II Maintenance 6.3. Refill / replace Reagents The liquid level in the containers is monitored. The following mes- sage is displayed: Container almost Maintenance E065 - Reagents low and the empty remaining reagent volume in% (starting at 17% = 340ml). See Operation, S.
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AMI Phosphate-II Maintenance WARNING Read the warnings for each chemical carefully.Observe the necessary security measures when handling dangerous chemi- cals. Wear suitable protective clothing, gloves and eye/face pro- tection. In case of accident or if you feel unwell, seek medical advice immediately (show the label where possible).
AMI Phosphate-II Maintenance 6.4. Verification The “Verification kit for AMI Photometer” is available as an accessory. An optical window with a precisely determined absorbance value is placed into the light beam of the pho- tometer. The actual measured absorbance will be compared to the reference value labeled on each kit.
AMI Phosphate-II Maintenance 6.5. Calibration Select Menu 3.1 (Maintenance/Calibration) and follow the instruc- tions on the display. Calibration Calibration 3.1.1 3.1.1 Close sample tap - Fill flow cell with standard - prepare 1 liter of standard. Standard: 1.00 ppm Enter Wait for next prompt <Enter>...
AMI Phosphate-II Maintenance 6.6. Cleaning the protective Filter Switch off the instrument according to instructions in Stop of Opera- tion for Maintenance, S. 40 Flow cell block Flow regulating valve Filter shaft Filter Filter vessel Normally the filter in your sample supply line will retain most debris.
AMI Phosphate-II Maintenance 6.7. Cleaning the Photometer Clean the photometer after indication by alarm (E020, FOME dirty). Switch off the instrument according to instructions in Stop of Opera- tion for Maintenance, S. Material Small brush. Procedure Flow regulating valve Photometer cover...
AMI Phosphate-II Maintenance 6.8. Cleaning the Flow Cell Because of using molybdenum, the flow cell block and the tubes will change color. Use 10% ammonia to remove the blue color. ATTENTION Never use organic solvents or scrubbing materials to clean acrylic glass parts.
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AMI Phosphate-II Maintenance WARNING Fragile; handle with care. Cleaning 1 Switch off the instrument according to instructions in Stop of Operation for Maintenance, S. 40 2 Remove the constant head cover [A]. 3 Pull the overflow tube [B] out of the flow cell block [D] 4 Remove the outer tube [C] from the flow cell block.
AMI Phosphate-II Maintenance 6.8.2 Assemble the Flow Cell Constant head cover Overflow tube Outer tube Gaskets Flow cell block Flow regulating valve Level 1 Replace all gaskets [D] before reassembling the flow cell. Note: A film of teflon paste (e.g. Fomblin from Solvay Solexis) on the gaskets improves tightness and life time.
AMI Phosphate-II Maintenance 6.9. Cleaning the solenoid valve Disassemble The solenoid valve is mounted below the constant head. The sole- noid valve should be disassembled if it does not switch anymore or the solenoid if it is clogged. valve 1 Switch off the instrument according to instructions in Stop of Operation for Maintenance, S.
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AMI Phosphate-II Maintenance Note: The O-rings inside the valve body may stick on the flow cell and fall down if the valve body is removed. 5 Remove the valve body from the flow cell. 6 Remove the white plate (G) with a screw driver size 0 (F).
AMI Phosphate-II Maintenance 6.10. Tube Replacement 6.10.1 Changing Pump Tubes The pump tubes [D] of the peristaltic pump are exposed to a mini- mal wear. It is therefore recommended to exchange the pump tubes annually. Pump housing Occlusion frames closed...
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AMI Phosphate-II Maintenance Dismount The pump tubes can easily be dismounted and mounted. pump tubes Proceed as follows: WARNING Shut off power before removing the pump tubes. 1 Switch off the instrument according to instructions in Stop of Operation for Maintenance, S. 40...
AMI Phosphate-II Maintenance 6.11. Replacing Fuses WARNING Beware of electrical shock. Disconnect the instrument and devices connected to: Relay 1 Relay 2 Alarm relay from the mains before opening the cover. Find and repair the cause for the short circuit before replacing the fuse.
AMI Phosphate-II Maintenance 6.12. Longer Stop of Operation 1 Switch off the instrument according to instructions in Stop of Operation for Maintenance, S. 40 2 Open pump tube assembly of Peristaltic pumps. Changing Pump Tubes, S. 52 3 Empty the filter vessel.
AMI Phosphate-II Error List Error List Error Non-fatal Error. Indicates an alarm if a programmed value is ex- ceeded. Such Errors are marked E0xx (bold and black). Fatal Error (blinking symbol) Control of dosing devices is interrupted. The indicated measured values are possibly incorrect.
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AMI Phosphate-II Error List Error Description Corrective action – check process E001 Phos. 1 Alarm high – check programmed value 5.3.1.1.x.1, S. 76 – check process E002 Phos. 1 Alarm low – check programmed value 5.3.1.1.x.2x, S. 76 – check process E003 Phos.
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AMI Phosphate-II Error List Error Description Corrective action – check control device or programming in E017 Control Timeout Installation, Relay contact, Relay 1/2 5.3.2/3, S. 77 – shut off power E018 Reagent Pump – check wiring – shut off power...
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AMI Phosphate-II Error List Error Description Corrective action – Check 2 sample stream option E034 Sample Flow 2 low – none, normal status E049 Power-on – none, normal status E050 Power-down E065 Reagents low Observe the decreasing number on the display, indicating for how many hours the reagents last.
AMI Phosphate-II Program Overview Program Overview For explanations about each parameter of the menus see Program List and Explanations, S. 70 Menu 1 Messages is always accessible for everybody. No password protection. No settings can be modified. Menu 2 Diagnostics is always accessible for everybody. No password protection.
AMI Phosphate-II Program Overview 8.2. Diagnostics (Main Menu 2) Identification Desig. AMI Phosphate-II B * Menu numbers 2.1* Version V5.01 - 03/12 Peripherals PeriClip 1 1.03 2.1.3.1* 2.1.3* PeriClip 2 1.03 If cleaning Module is installed Factory Test Instrument 2.1.4.1* 2.1.4*...
AMI Phosphate-II Program Overview 8.5. Installation (Main Menu 5) Sensors Ref. Verification 5.1.1* * Menu numbers 5.1* Phosphate as 5.1.2* Standard PO4 5.1.3* Meas. Interval 5.1.4* Channels 5.1.5* Channel Selection 5.1.6* Signal Outputs Signal Output 1/2 Parameter 5.2.1.1/5.2.2.1* 5.2* 5.2.1*/5.2.2* Current Loop 5.2.1.2/5.2.2.2*...
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AMI Phosphate-II Program Overview Miscellaneous Language 5.4.1* 5.4* Set defaults 5.4.2* Load Firmware 5.4.3* Password Messages 5.4.4.1* 5.4.4* Maintenance 5.4.4.2* Operation 5.4.4.3* Installation 5.4.4.4* Sample ID 5.4.5* Interface Protocol 5.5.1* (only with RS485 5.5* Device Address 5.5.21* or RS232 interface) Baud Rate 5.5.31*...
AMI Phosphate-II Program List and Explanations Program List and Explanations 1 Messages 1.1 Pending Errors 1.1.5 Provides the list of active errors with their status (active, acknowl- edged). If an active error is acknowledged, the alarm relay opens again. Cleared errors are moved to the Message list.
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AMI Phosphate-II Program List and Explanations 2.2.1.5 Ver. History: Review verifications values of the last verifications: 2.2.1.5.1 Number: Verification counter Date, Time: Date and time of verification Absorbance: Measured absorbance of the reference kit. Reference value: True value of the reference kit according to label.
AMI Phosphate-II Program List and Explanations 3 Maintenance 3.1 Calibration 3.1.5 Calibration: Performs a calibration using the standard soluti- non.Follow dialog on the screen.See Calibration, S. 44 3.2 Service 3.2.1 Verification: Performs a verification using the reference kit. Follow dialog. See Verification, S.
AMI Phosphate-II Program List and Explanations 3.5 Cleaning Automatic cleaning process using Cleaning module-II (optional) controlled by transmitter of AMI Phosphate-II. – Measurement is interrupted. – Flow error interrupts cleaning. – Cleaning does not start: E022 Reagent empty, E023 Cleaning solution, no flow.
AMI Phosphate-II Program List and Explanations 4 Operation 4.1 Sensors 4.1.1 Filter Time Constant: Used to damp noisy signals. The higher the filter time constant, the slower the system reacts to changes of the measured value. Range: 5–300 sec 4.1.2 Hold after Cal: Delay permitting the instrument to stabilize again af- ter calibration.
Mode Internal: In this mode, the AMI Phosphate-II B sequentially measures each sample stream of the second stream option. Mode External: In this mode, the AMI Phosphate-II B can be con- trolled via signal input. Mode Fieldbus: The AMI Phosphate-II B is controlled via fieldbus 5.1.7...
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AMI Phosphate-II Program List and Explanations 5.2.1.3-5.2.2.3 Function: Define if the signal output is used to transmit a process value or to drive a control unit. Available functions are: Linear, bilinear or logarithmic for process values. As process values, S. 73 ...
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AMI Phosphate-II Program List and Explanations As control out- Signal outputs can be used for driving control units. We distinguish different kinds of controls: P-controller: The controller action is proportional to the devi- ation from the setpoint. The controller is characterized by the P-Band.
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AMI Phosphate-II Program List and Explanations Control Setpoint: User-defined process value (Measured value or flow) Range: 0–10 ppm upwards/ downwards P-Band: Range below (upwards control) or above (downwards con- trol) the set-point, within the dosing intensity is reduced from 100% to 0% to reach the set-point without overshooting.
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AMI Phosphate-II Program List and Explanations 5.3.1.1.x.1 Alarm High: If the measured value rises above the alarm high val- ue, the alarm relay is activated and E001 is displayed in the mes- sage list. Range: 0.00–10.00 ppm 5.3.1.1.x.2x Alarm Low: If the measured value falls below the alarm low value, the alarm relay is activated and E002 is displayed in the message list.
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AMI Phosphate-II Program List and Explanations 5.3.2/3 Relay 1/2: The function of relay contacts 1 or 2 are defined by the user 1 First select the functions as: - limit switch, Limit upper / lower, S. 77 - controller, Control upwards / downwards, S. 77 - timer or Timer, S.
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AMI Phosphate-II Program List and Explanations 5.3.2.32.30 Response time: Minimal time the metering device needs to react. Range: 0–240 sec. Frequency Examples of metering devices that are puls frequency driven are the classic membrane pumps with a potential free triggering input.
AMI Phosphate-II Program List and Explanations 5.3.4 Input: The functions of the relays and signal outputs can be de- fined depending on the position of the input contact, i.e. no function, closed or open. 5.3.4.1 Active: Define when the input should be active: Input is never active.
AMI Phosphate-II Program List and Explanations 5.4 Miscellaneous 5.4.1 Language: Set the desired language. Available settings: German / English / French / Spanish / Italian 5.4.2 Set defaults: Reset the instrument to factory default values in three different ways: Calibration: Sets calibration values back to default. All oth- er values are kept in memory.
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AMI Phosphate-II Program List and Explanations 5.5 Interface Select one of the following communication protocols. Depending on your selection, different parameters must be defined. 5.5.1 Protocol: Profibus 5.5.20 Device address: Range: 0–126 5.5.30 ID No.: Range: Analyzer; Manufacturer; Multivariable 5.5.40...
AMI Phosphate-II Material Safety Data sheets Material Safety Data sheets 10.1. OXYCON ON-LINE phosphate reagent 1 1 Identification of the substance/preparation and of the company/undertaking Identification of the product Catalogue No.: Included in A-85.420.660 Product name: OXYCON ON-LINE phosphate reagent 1 Use of substance/preparation Reagent for analysis.
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AMI Phosphate-II Material Safety Data sheets 6 Accidental release measures Procedures for cleaning / absorption: Take up dry. Forward for disposal. Clean up affected area 7 Handling and storage Handling: No further requirements Storage: Tightly closed and dry at room temperature (+15 °C to +25 °C)
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AMI Phosphate-II Material Safety Data sheets 10 Stability and reactivity Conditions to be avoided: No information available Substances to be avoided: No information available Hazardous decomposition products: Ammonia 11 Toxicological information Subacute to chronic toxicity Bacterial mutagenicity: Escherichia coli: Negative...
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AMI Phosphate-II Material Safety Data sheets 15 Regulatory information Labeling according to EC Directives Symbol: R-phrases: S-phrases: 16 Other information Date of issue: 01.10.2009 The information contained herein is based on the present state of our knowledge. It characterizes the product with regard to the appropriate safety precautions. It does not represent a guarantee of the properties of the product.
AMI Phosphate-II Material Safety Data sheets 10.2. OXYCON ON-LINE phosphate reagent 2 1 Identification of the substance/preparation and of the company/undertaking Identification of the product Catalogue No.: Included in A-85.420.660 Product name: OXYCON ON-LINE phosphate reagent 2 Use of substance/preparation Reagent for analysis.
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AMI Phosphate-II Material Safety Data sheets 5 Fire-fighting measures Suitable extinguishing media: In adaptation to materials stored in the immediate neighborhoods 6 Accidental release measures Person-related precautionary measures: Do not inhale vapors / aerosols. Ensure supply of fresh air in enclosed rooms...
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AMI Phosphate-II Material Safety Data sheets 10 Stability and reactivity Conditions to be avoided: No information available Substances to be avoided: Strong oxidizing agents Hazardous decomposition products: No information available 11 Toxicological information Acute toxicity LD50 (oral, rat): 115mg/ kg (pure hazardous ingredients)
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AMI Phosphate-II Material Safety Data sheets 15 Regulatory information Labeling according to EC Directives Symbol: R-phrases: 20/22 Harmful by inhalation and if swallowed S-phrases: 16 Other information Date of issue: 01.10.2009 The information contained herein is based on the present state of our knowledge. It characterizes the product with regard to the appropriate safety precautions.
AMI Phosphate-II Default Values Default Values Operation: Sensors: Filter Time Const.:..............30 Sec Hold after Cal.: ..............300 Sec Alarm Relay ..............same as in Installation Signal Output ..............same as in Installation Relay 1/2 ..............same as in Installation Input ..............same as in Installation Logger: Logger Interval:............
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AMI Phosphate-II Default Values Relay1/2 Function:................limit upper Parameter:..............Phosphate 1 Setpoint: ................10.0 ppm Hysteresis:................. 0.10 ppm Delay: ..................30 Sec If Function = Control upw. or dnw: Parameter:..............Phosphate 1 Settings: Actuator: ............Frequency Settings: Pulse Frequency:............. 120/m Settings: Control Parameters: Setpoint: ......
AMI Phosphate II Index Index ....Alarm Relay occlusion frames ..On site requirements option ..cleaning module ..Cable thicknesses second sample stream .
AMI Phosphate-II Notes Notes A-96.250.641 / 290312...
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AMI Phosphate-II SWAN is represented worldwide by subsidiary companies and distributors. cooperates with independent representatives all over the world. SWAN Products Analytical Instruments for: High Purity Water Feedwater, Steam and Condensate Potable Water Pool and Sanitary Water Cooling Water Waster Water and Effluents Made in Switzerland A-96.250.641 / 290312...
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