Related Manuals for Foss Soxtec 1047
Summary of Contents for Foss Soxtec 1047
- Page 1 ® Soxtec 1047 System Hydrolyzing Unit User Manual 1000 3315 / Rev. 2.2 1047011b Copyright 2001/ All rights reserved FOSS TECATOR AB, Box 70, S-26321 Höganäs, Sweden Tel Int +46 42 361500, Fax +46 42 343150...
- Page 3 Dansk Teksten med sikkerhedsinformation er skrevet i denne stil og oversat til de lokale sprog (EU/EES). Informationen kan findes på de gule sider. Deutsch Text über Sicherheitsinformationen ist in diesem Stil geschrieben und in andere Sprachen (EU/EES) übersetzt. Die Informationen finden sich auf den gelben Seiten.
- Page 4 Nederlands De tekst inzake veiligheidsvoorschriften is in het opgesteld en wordt in het Nederlands vertaald. De informatie staat in de gouden gids. Norsk Tekst som gjelder sikkerhetsinformasjon er skrevet med denne stilen og er oversatt til lokalt språk (EU/EES). Informasjonen finnes på de gule sidene. Português O texto sobre as informações de segurança está...
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Page 5: Table Of Contents
............12 Change of fuses ..................12 TECHNICAL SPECIFICATIONS Safety ......................13 Environmental conditions ...............13 Lifting instructions ................13 Foss Tecator APPLICATION NOTES SYSTEM ACCESSORIES AND SPARE PARTS Accessories ....................15 Spare parts ....................15 Manufacturer’s name and address ..........15 SAFETY INFORMATION 1047 (GB) ........17 SICHERHEITSINFORMATIONEN 1047(DE) ....20... - Page 6 TURVALLISUUSOHJEET 1047 (FIN) ........32 INSTRUCTIONS DE SECURITE 1047(FR) ....36 ËÇØÇ ÌÅÔÑÙÍ ÁÓÖÁËÅÉÁÓ 1047 (GR) ......40 ÖRYGGISLEIÐBEININGAR 1047(IS) ......45 INFORMAZIONI DI SICUREZZA 1047(IT) ....48 VEILIGHEIDSINFORMATIE 1047(NL) ......52 SIKKERHETSINFORMASJON 1047(NO) .....56 INFORMAÇÕES DE SEGURANÇA 1047(PT) ...59 SÄKERHETSINFORMATION 1047(SE) ......63...
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Page 7: Precautions And Procedures 1.1 Intended Use
The 1047 Hydrolyzing Unit is designed for laboratory use analysing parameters as specified in Foss Tecators Application Notes. Please read these operating instructions carefully and act accordingly. For safety reasons people not familiar with these operating instructions must not use the... -
Page 9: Introduction
INTRODUCTION Crude Fat is generally defined as sample constituents soluble in appropriate organic solvents, such as diethyl ether, petroleum ether or chloroform. The main constituents in Crude Fat are triglycerols and free fatty acids. In certain Sample types, however, some of the fat, or lipids, are bound as lipoproteins, liposaccharides or metal salts. -
Page 10: Preparations For Use
Remove all packing material. Use the parts list, packed together with the instrument and check that you have received all parts. Use Fig.2 to identify the different parts. If any parts are missing, contact your Foss Tecator representative. 1047011A Fig. 2 1. -
Page 11: Installation
Installation All text in this section is translated in local language. Installation requirements 3.2.1 Power supply 110 or 200-230V, 50-60 Hz Power consumption 975W Dimensions L x D x H 61 x 31 x 85 cm Weight 23 kg Water supply Tap water approx. -
Page 12: Operation
1047 Hydrolyzing Unit in conjunction with 1043 or 1045 Soxtec Extraction Systems, is generally based. For more detailed information on specific types of samples, please ask your local Foss Tecator dealer for "Application Notes". Preliminary preparation In order to achieve as good results as possible, all samples must be homogenized in a proper way before chemical treatment. -
Page 13: Pre-Extraction
Pre-extraction As high fat levels can prevent effective hydrolysis, samples with 10% fat content should be pre-extracted with the same type of solvent as used in the final extraction. 1.Weight in the sample with a precision of 1000 ±2 mg. Load the glass thimble with 1 g celite and the sample. -
Page 14: Hydrolysis
Hydrolysis Weigh the samples with a precision of 1000 ±2 mg and transfer them to the sample tubes. Add 1-2 g of celite and 100-120 ml of the acid solution to each sample tube. The level of the acid solution must be over the top of the cover of the heaters. -
Page 15: Drying
11. Wash each tube by opening the vacuum valve and spray 5x50 ml of approximately 50°C distilled water, by using the water sprayer (Fig. 9). 12. Raise the suction tubes and take out one of the sample tubes. Cover the cleaning rod with a thin layer of defatted cottonwool and wet it with acetone. -
Page 16: Calculation
Calculation Calculate the fat content according to the formula below. W3 = The extraction cup weight after fat extraction and cooling in desiccator. W2 = Clean and predried extraction cup. W1 = Sample weight. W3-W2 % Fat x 100 If a pre-extraction was required, using two extraction cups, add the two results that have been calculated, and the sum is the total fat in the sample. -
Page 17: Maintenance
MAINTENANCE Change of vacuum valve Loosen all neoprene tubings carefully that are connected to the suction tubes, by removing the plastic straps. Lower the suction tubes down the horizontal plate, so the suction tubes rest against the bottom of the oven. Unscrew the 3 screws that are placed on the white plate on the backside of the hydrolyzing unit. -
Page 18: Change Of The Lower Thimble Holder
2. Carefully loosen and pull out the old filter seal. Press gently down the new filter seal. Note: Check carefully the correct positioning of the new filter seals. Change of the lower thimble holder 1. Loosen the old thimble holder by gently easing and pulling it upwards. -
Page 19: Technical Specifications
TECHNICAL SPECIFICATIONS Safety The insulation of external, inaccessible circuits is reinforced. Environmental conditions The equipment is designed to be safe at least under the following conditions: · Indoor use · Altitude up to 2000 m. · Temperature 5°C to 40°C. ·... -
Page 20: Foss Tecator Application Notes System
Extraction (with hydrolysis) method. please see the Application Note AN 301. In Foss Tecators extensive list of Application Sub Notes you will find information on how to analyse the sample of your choice. Please contact your Foss Tecator representative for more details. -
Page 21: Accessories And Spare Parts
1565 0026 Mains cable 110V 1565 0063 Fuse T 6,3 A 1564 0083 Fuse 10 A 1564 0006 Manufacturer’s name and address Foss Tecator AB Box 70 S-263 21 Höganäs Sweden Int phone. +46 42 361500 Int fax. +46 42 340349... - Page 24 2. Add 1-2 g of celite and 100-120 ml of the sample solution and as much as possible of 9.4.2 Pre-extraction 9.4.5 Solvent extraction acid solution to each sample tube. The level the solid particles in the solution. Close the As high fat levels can prevent effective of the acid solution must be over the top of valve and repeat in the same way with the...
- Page 25 3. Unscrew the 3 screws that are placed on the 4. Cooling water inlet TECHNICAL white plate on the backside of the 2. Carefully loosen and pull out the old filter 5. Drain SPECIFICATIONS hydrolyzing unit. Unscrew the 3 screws that seal.
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