HP 5890 Series II Plus Reference Manual page 226

Test Sample Chromatograms
Test sample chromatograms
Figure 10-2.
Detector Type NPD (or NPDw/MUG)
Temp 220 DEGREES C
Inlet Type PACKED (OR PURGED
PACKED).
Temp 170 DEGREES C
Operating Mode
Purge Time On
Purge Time Off
Oven Isothermal
Init Temp
Init Time
Ramp
Rate
Fin Temp
Fin Time
Range 0
COLUMN:
Part No. 19095S(#100)
Dimensions
Sta Phase Methyl Silicone
Nitrogen-Phosphorus Detector (NPD)
226
HP 5890 Test Sample Operating
Conditions
N/A
N/A min
N/A min
170 DEGREES C
3.0 min
0
¿
530 MID; 5 M
IF
START
IF
IF
ST
FLOW RATES
Carrier (He) 20 +/• 1
Hydrogen 3.5 +/• 0.1
Air 100•120 +/• 10 ml/min
Makeup (He) 10+/•1
Split Vent
Septum Purge
SAMPLE:
Type NP-FID Sample
¿
Inj Volume 3
Part No. 18789•60060
Composition 0.65 ppm azobenzene,
100 ppm octadecane, 1.0 ppm
malathion in isooctane
AZOBENZENE
.659
C18
MALATHION
2.138
ml/min
ml/min
ml/min
N/A ml/min
1•2 ml/min
l